Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Understanding the Effect of Electron Beam Melting Scanning Strategies on the Aluminum Content and Materials State of Single Ti-6Al-4V Feedstock

Journal Article · · Materials
DOI:https://doi.org/10.3390/ma16196366· OSTI ID:2469811
 [1];  [2];  [3]
  1. Iowa State University, Ames, IA (United States); Ames Laboratory (AMES), Ames, IA (United States); Carnegie Mellon University, Pittsburgh, PA (United States)
  2. Iowa State University, Ames, IA (United States)
  3. Iowa State University, Ames, IA (United States); Ames Laboratory (AMES), Ames, IA (United States)
Research on the additive manufacturing of metals often neglects any characterization of the composition of final parts, erroneously assuming a compositional homogeneity that matches the feedstock material. Here, the composition of electron-beam-melted Ti-6Al-4V produced through three distinct scanning strategies (linear raster and two point melting strategies, random fill and Dehoff fill) is characterized both locally and globally through energy-dispersive spectroscopy and quantitative chemical analysis. As a result of the different scanning strategies used, differing levels of preferential vaporization occur across the various parts, leading to distinct final compositions, with extremes of ~5.8 wt.% Al and ~4.8 wt.% Al. In addition, energy-dispersive spectroscopy composition maps reveal specific features in both the XY and XZ planes (with Z being the build direction) as a result of local inhomogeneous preferential vaporization. The subsequent change in composition significantly modifies the materials’ state of parts, wherein parts and local regions with higher aluminum contents lead to higher hardness levels (with a ~50 HV difference) and elastic property values and vice versa. While varying scan strategies and scan parameters are known to modify the microstructure and properties of a part, the effect on composition cannot, and should not, be neglected.
Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
Office of Naval Research (ONR); USDOE
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
2469811
Journal Information:
Materials, Journal Name: Materials Journal Issue: 19 Vol. 16; ISSN 1996-1944
Publisher:
MDPICopyright Statement
Country of Publication:
United States
Language:
English

References (39)

Additive Manufacturing of Titanium Alloys by Electron Beam Melting: A Review journal December 2017
Precise Measurements of Thermophysical Properties of Liquid Ti–6Al–4V (Ti64) Alloy On Board the International Space Station journal April 2020
Building new entities from existing titanium part by electron beam melting: microstructures and mechanical properties journal November 2015
3D characterization of microstructural evolution and variant selection in additively manufactured Ti-6Al-4 V journal June 2021
Using defects as a ‘fossil record’ to help interpret complex processes during additive manufacturing: as applied to raster-scanned electron beam powder bed additively manufactured Ti–6Al–4V journal August 2023
Texture Analysis of Additively Manufactured Ti-6Al-4V Deposited Using Different Scanning Strategies journal October 2020
Evaluation of evaporation losses during electron-beam melting of Ti-Al-V alloys journal December 2003
Recyclability Study on Inconel 718 and Ti-6Al-4V Powders for Use in Electron Beam Melting journal October 2015
Strategy for Texture Management in Metals Additive Manufacturing journal January 2017
Predicting tensile properties of Ti-6Al-4V produced via directed energy deposition journal July 2017
Design of titanium alloys by additive manufacturing: A critical review journal January 2022
Additive manufacturing of magnesium alloys journal March 2020
Additive manufacturing (3D printing): A review of materials, methods, applications and challenges journal June 2018
Metal additive manufacturing in structural engineering – review, advances, opportunities and outlook journal January 2023
First-principles study of the phase stability and elastic properties of Ti-X alloys (X = Mo, Nb, Al, Sn, Zr, Fe, Co, and O) journal December 2017
In-situ alloying in laser-based additive manufacturing processes: A critical review journal August 2021
Additive manufacturing of Ti6Al4V alloy: A review journal February 2019
High-throughput synthesis of Mo-Nb-Ta-W high-entropy alloys via additive manufacturing journal February 2020
The effect of beam scan strategies on microstructural variations in Ti-6Al-4V fabricated by electron beam powder bed fusion journal November 2020
Five-parameter characterization of intervariant boundaries in additively manufactured Ti-6Al-4V journal November 2020
Metal additive manufacturing in aerospace: A review journal November 2021
Additive manufacturing of functionally graded materials: A review journal September 2019
Additive manufacturing of structural materials journal July 2021
Influence of scan strategy on porosity and microstructure of Ti-6Al-4V fabricated by electron beam powder bed fusion journal September 2020
Formation and 3D morphology of interconnected α microstructures in additively manufactured Ti-6Al-4V journal December 2021
Spherical pores as ‘microstructural informants’: Understanding compositional, thermal, and mechanical gyrations in additively manufactured Ti-6Al-4V journal June 2021
3D electron backscatter diffraction study of α lath morphology in additively manufactured Ti-6Al-4V journal November 2020
Additive manufacturing of metallic components by selective electron beam melting — a review journal March 2016
Microstructural and Mechanical Property Differences Resulting from Melt Pool Interactions with the Electron Beam Chamber Environment journal July 2023
Comparison of density measurement techniques for additive manufactured metallic parts journal August 2011
Material-structure-performance integrated laser-metal additive manufacturing journal May 2021
Microstructural Control of Additively Manufactured Metallic Materials journal July 2016
Site specific control of crystallographic grain orientation through electron beam additive manufacturing journal November 2014
Kinetics of Evaporation of Alloying Elements under Vacuum: Application to Ti alloys in Electron Beam Melting journal September 2017
Additive Manufacturing for Aerospace Flight Applications journal September 2016
Differences in Defect Distribution Across Scan Strategies in Electron Beam AM Ti-6Al-4V journal July 2021
Effects of Gas Pressure during Electron Beam Energy Deposition in the EBM Additive Manufacturing Process journal April 2021
Influence of Aluminum and Copper on Mechanical Properties of Biocompatible Ti-Mo Alloys: A Simulation-Based Investigation journal May 2023
Chemistry Control in Electron Beam Deposited Titanium Alloys journal April 2009

Similar Records

Analysis of multicomponent evaporation in electron beam melting and refining of titanium alloys
Journal Article · Mon Dec 01 04:00:00 UTC 1997 · Metallurgical and Materials Transactions B: Process Metallurgy and Materials Processing Science · OSTI ID:585999

Fundamental cosmology from ANDES precision spectroscopy
Journal Article · Fri May 05 00:00:00 UTC 2023 · Monthly Notices of the Royal Astronomical Society · OSTI ID:1974254

Crustal-thickness variations in the central Andes
Journal Article · Wed May 01 04:00:00 UTC 1996 · Geology · OSTI ID:420917