Operando methods: A new era of electrochemistry

Yang, Yao; Feijóo, Julian; Briega-Martos, Valentín; Li, Qihao; Krumov, Mihail; Merkens, Stefan; De Salvo, Giuseppe; Chuvilin, Andrey; Jin, Jianbo; Huang, Haowei; Pollock, Christopher J.; Salmeron, Miquel B.; Wang, Cheng; Muller, David A.; Abruña, Héctor D.; Yang, Peidong

doi:10.1016/j.coelec.2023.101403

Operando methods: A new era of electrochemistry

Journal Article · Thu Sep 28 00:00:00 EDT 2023 · Current Opinion in Electrochemistry

DOI:https://doi.org/10.1016/j.coelec.2023.101403· OSTI ID:2467424

^[1]; ^[2]; ^[3]; ^[4]; ^[4]; ^[5]; ^[5]; ^[6]; ^[7]; Huang, Haowei ^[7]; Pollock, Christopher J. ^[8]; Salmeron, Miquel B. ^[9]; ^[10]; Muller, David A. ^[4]; Abruña, Héctor D. ^[4]; Yang, Peidong ^[11]

University of California, Berkeley, CA (United States); Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States); Cornell Univ., Ithaca, NY (United States)
University of California, Berkeley, CA (United States); Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)
Forschungszentrum Juelich, Erlangen (Germany). Helmholtz-Institute Erlangen-Nürnberg for Renewable Energy (IEK-11)
Cornell Univ., Ithaca, NY (United States)
CIC NanoGUNE BRTA, Donostia (Spain). Electron Microscopy Laboratory
CIC NanoGUNE BRTA, Donostia (Spain). Electron Microscopy Laboratory; Basque Foundation for Science, Bilbao (Spain). IKERBASQUE
University of California, Berkeley, CA (United States)
Cornell Univ., Ithaca, NY (United States). Cornell High Energy Synchrotron Source (CHESS)
Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States); University of California, Berkeley, CA (United States)
Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States). Advanced Light Source (ALS)
University of California, Berkeley, CA (United States); Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States); Cornell Univ., Ithaca, NY (United States). Cornell High Energy Synchrotron Source (CHESS); Kavli Energy NanoScience Institute, Berkeley, CA (United States)

One of the grand challenges facing electrochemistry is to directly resolve the complex nature of (electro)catalyst active sites and capture real-time “movies” of reaction dynamics, i.e. “watching chemistry in action”. The need for such fundamental understanding has stimulated the development of operando/in situ methods, which have greatly enhanced our ability to identify activity descriptors of electrocatalysts and establish structure–property relationships of energy materials. Here, this review summarizes the frontiers of operando electrochemical liquid-cell scanning transmission electron microscopy and correlative synchrotron X-ray methods, which are complementary tools to comprehensively investigate reaction dynamics across multiple spatiotemporal scales. In an effort to encourage greater adoption of advanced operando methods by the general electrochemistry community, this review points out the need to benchmark electrochemistry in confined and heterogenous liquid environment with minimal beam-induced damage. We anticipate that multimodal operando methods will become indispensable for understanding interfacial reaction mechanisms for the broad chemistry and energy materials communities.

View Accepted Manuscript (DOE)

Research Organization:: Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)

Sponsoring Organization:: National Science Foundation (NSF); USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division (CSGB); USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities (SUF)

Grant/Contract Number:: AC02-05CH11231; SC0019445

OSTI ID:: 2467424

Journal Information:: Current Opinion in Electrochemistry, Journal Name: Current Opinion in Electrochemistry Vol. 42; ISSN 2451-9103

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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