Insights into Heterogeneous Catalysts under Reaction Conditions by In Situ/Operando Electron Microscopy

Cheng, Han‐Wen; Wang, Shan; Chen, Guanyu; Liu, Zhengwang; Caracciolo, Dominic; Madiou, Merry; Shan, Shiyao; Zhang, Jincang; He, Heyong; Che, Renchao; Zhong, Chuan‐Jian

doi:10.1002/aenm.202202097

Insights into Heterogeneous Catalysts under Reaction Conditions by In Situ/Operando Electron Microscopy

Journal Article · Sun Aug 21 00:00:00 EDT 2022 · Advanced Energy Materials

DOI:https://doi.org/10.1002/aenm.202202097· OSTI ID:2419712

Cheng, Han‐Wen ^[1]; Wang, Shan ^[2]; Chen, Guanyu ^[3]; Liu, Zhengwang ^[3]; Caracciolo, Dominic ^[2]; Madiou, Merry ^[2]; Shan, Shiyao ^[2]; Zhang, Jincang ^[4]; He, Heyong ^[3]; ^[5]; ^[2]

Fudan Univ., Shanghai (China); State Univ. of New York (SUNY), Binghamton, NY (United States); OSTI
State Univ. of New York (SUNY), Binghamton, NY (United States)
Fudan Univ., Shanghai (China)
Zhejiang Laboratory (China)
Fudan Univ., Shanghai (China); Zhejiang Laboratory (China)

The advancement of clean energy and environment depends strongly on the development of efficient catalysts in a wide range of heterogeneous catalytic reactions, which has benefited from transmission electron microscopic techniques in determining the atomic-scale morphologies and structures. However, it is the morphology and structure under the catalytic reaction conditions that determine the performance of the catalyst, which has captured a surge of interest in developing and applying in situ/operando transmission electron microscopic techniques in heterogeneous catalysis. The major theme of this review is to highlight some of the most recent insights into heterogeneous catalysts under the relevant reaction conditions using in situ/operando transmission electron microscopic techniques. Rather than a comprehensive overview of the basic principles of in situ/operando techniques, this review focuses on the insights into the atomic-scale/nanoscale details of various catalysts ranging from single-component to multicomponent catalysts under heterogeneous catalytic, electrocatalytic, and photocatalytic reaction conditions involving both gas–solid and liquid–solid interfaces. Here, this focus is coupled with discussions of the correlation of the atomic, molecular, and nanoscale morphology, composition, and structure with the catalytic properties under the reaction conditions, shining light on the challenges and opportunities in design of nanostructured catalysts for clean and sustainable energy applications.

View Accepted Manuscript (DOE)

Research Organization:: Central Michigan Univ., Mount Pleasant, MI (United States)

Sponsoring Organization:: USDOE; USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: SC0006877

OSTI ID:: 2419712

Alternate ID(s):: OSTI ID: 1892353

Journal Information:: Advanced Energy Materials, Journal Name: Advanced Energy Materials Journal Issue: 38 Vol. 12; ISSN 1614-6832

Publisher:: WileyCopyright Statement

Country of Publication:: United States

Language:: English

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