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Methods for the production of cathode materials for lithium ion batteries

Patent ·
OSTI ID:2294019

The present disclosure provides methods for producing cathode materials for lithium ion batteries. Cathode materials that contain manganese are emphasized. Representative materials include LixNi1−y−zMnyCozO2 (NMC) (where x is in the range from 0.80 to 1.3, y is in the range from 0.01 to 0.5, and z is in the range from 0.01 to 0.5), LixMn2O4 (LM), and LixNi1−yMnyO2 (LMN) (where x is in the range from 0.8 to 1.3 and y is in the range from 0.0 to 0.8). The process includes reactions of carboxylate precursors of nickel, manganese, and/or cobalt and lithiation with a lithium precursor. The carboxylate precursors are made from reactions of pure metals or metal compounds with carboxylic acids. The manganese precursor contains bivalent manganese and the process controls the oxidation state of manganese to avoid formation of higher oxidation states of manganese.

Research Organization:
Ge Solartech, LLC, Troy, MI (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
SC0017761
Assignee:
Ge Solartech, LLC (Troy, MI)
Patent Number(s):
11,855,281
Application Number:
17/693,330
OSTI ID:
2294019
Country of Publication:
United States
Language:
English

References (1)

Sol–gel synthesis of sodium and lithium based materials journal June 2012

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