skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Influence of TiH{sub 2} on Interfacial Reaction Features Between Cubic Boron Nitride and Cu-Sn-Ti Active Filler Metals

Journal Article · · Metallurgical and Materials Transactions. B, Process Metallurgy and Materials Processing Science
; ;  [1]
  1. Northeastern University, School of Metallurgy (China)

Cubic boron nitride (CBN) grains are brazed by Cu-Sn-Ti filler metal in vacuum at 1223 K. Wetting behaviors, reaction layer features, and elemental distribution characteristics have been systematically investigated through scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and X-ray diffraction (XRD). The results show that when the TiH{sub 2} content is 5 wt pct, virtually no sharp-edged, partially coated, and uncoated CBN grains can be observed, indicating that adequate wetting could be achieved. Moreover, a continuous reaction layer with uniform thickness (1.30 μm) consisting of TiN, TiB{sub 2}, and TiB is obtained, which indicates that large numbers of TiN, TiB{sub 2}, and TiB compounds could have been formed at the interface. However, when the TiH{sub 2} content exceeds 5 wt pct, the thickness of the reaction layer is no longer significantly expanding and excessive Ti present in the matrix will lower the volume percentage of Cu{sub 3}Sn{sub 1} phase, which will reduce the bonding strength of the brazing samples. Wear tests indicate that the minimum weight loss also occurs at 5 wt pct TiH{sub 2}.

OSTI ID:
22933658
Journal Information:
Metallurgical and Materials Transactions. B, Process Metallurgy and Materials Processing Science, Vol. 50, Issue 2; Other Information: Copyright (c) 2019 The Minerals, Metals & Materials Society and ASM International; Country of input: International Atomic Energy Agency (IAEA); ISSN 1073-5615
Country of Publication:
United States
Language:
English

Similar Records

Optimizing Wear Resistance via Brazing Temperature Adaption: Application into CBN/Cu-Sn-Ti Composites
Journal Article · Sun Dec 15 00:00:00 EST 2019 · Metallurgical and Materials Transactions. B, Process Metallurgy and Materials Processing Science · OSTI ID:22933658

Effect of mechanical milling on Ni-TiH{sub 2} powder alloy filler metal for brazing TiAl intermetallic alloy: The microstructure and joint's properties
Journal Article · Thu Jan 15 00:00:00 EST 2009 · Materials Characterization · OSTI ID:22933658

Reaction layer characterization of the braze joint of silicon nitride to stainless steel
Journal Article · Sat Oct 01 00:00:00 EDT 1994 · Journal of Materials Engineering and Performance; (United States) · OSTI ID:22933658