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Combustion characteristics of diisopropoxymethane, a low-reactivity oxymethylene ether

Journal Article · · Fuel
 [1];  [2];  [2];  [2]
  1. Colorado State University, Fort Collins, CO (United States); United States Air Force Academy, CO (United States); Colorado State University
  2. Colorado State University, Fort Collins, CO (United States)
Oxymethylene ethers (OMEs) have been studied for use as low-sooting diesel fuel additives or substitutes; very little literature discusses OMEs as spark-ignition (SI) fuels due to their typically high cetane numbers. In this work, a lower-reactivity, branched OME, diisopropoxymethane (DIPM), is evaluated to determine its effectiveness as a spark-ignition fuel, as it is the lowest-reactivity OME (as determined by Indicated Cetane Number) thus far evaluated in the literature. DIPM is synthesized in-house via acetalization from isopropanol (iPrOH) and trioxane using standard OME production practices. DIPM was then tested in a rapid compression machine (RCM) for autoignition and spark ignition characteristics, and in a modified CFR engine to determine effective octane numbers. In the RCM, an autoignition temperature sweep was performed at stoichiometric conditions from 1000/T = 1.7 - 1.0, at 5:1 inert ratio (comparable to approximately 25% EGR), where it was found that DIPM has ignition delay times 5–10x faster than isooctane and displays NTC ignition behavior. Blends with iPrOH indicate that reactivity can be matched with isooctane with low blend ratios of iPrOH in DIPM. Flame speeds were tested with a laser spark for ignition in the RCM, where the flame speed of DIPM and isooctane is determined to be comparable at engine relevant conditions. In the CFR engine, effective RON and MON based on pressure trace frequency domain measurements were determined for DIPM and a 15 vol% iPrOH in DIPM blend. Neat DIPM has (R+M)/2 = 59 and a negative sensitivity of S = -18, consistent with its NTC behavior and higher reactivity. Furthermore the DIPM/iPrOH blend has positive sensitivity and a pump-gasoline range (R+M)/2 = 89.3. DIPM on its own is unlikely to be an effective SI fuel, however, when blended with iPrOH as an ON booster, it may be a promising SI candidate fuel.
Research Organization:
Colorado State University, Fort Collins, CO (United States)
Sponsoring Organization:
USDOE Office of Energy Efficiency and Renewable Energy (EERE), Office of Sustainable Transportation. Bioenergy Technologies Office (BETO)
Grant/Contract Number:
EE0008726
OSTI ID:
2283076
Journal Information:
Fuel, Journal Name: Fuel Vol. 362; ISSN 0016-2361
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English

References (41)

Influence of Silanol Defects of ZSM-5 Zeolites on Trioxane Synthesis from Formaldehyde journal November 2019
Potential of long-chain oxymethylene ether and oxymethylene ether-diesel blends for ultra-low emission engines journal April 2019
Combustion characteristics of a compression-ignition engine fuelled with diesel–dimethoxy methane blends under various fuel injection advance angles journal March 2006
Acetone-free biobutanol production: Past and recent advances in the Isopropanol-Butanol-Ethanol (IBE) fermentation journal September 2019
Reaction kinetics and equilibrium parameters for the production of oxymethylene dimethyl ethers (OME) from methanol and formaldehyde journal May 2017
Improved sooting tendency measurements for aromatic hydrocarbons and their implications for naphthalene formation pathways journal March 2007
The effect of diluent gases on ignition delay times in the shock tube and in the rapid compression machine journal October 2007
Nonlinear effects in the extraction of laminar flame speeds from expanding spherical flames journal September 2009
An experimental and kinetic modeling study of n-propanol and i-propanol ignition at high temperatures journal March 2014
Propanol isomers: Investigation of ignition and pyrolysis time scales journal February 2017
Pressure and temperature effects on fuels with varying octane sensitivity at high load in SI engines journal March 2017
End-gas autoignition fraction and flame propagation rate in laser-ignited primary reference fuel mixtures at elevated temperature and pressure journal December 2021
A study on fundamental combustion properties of oxymethylene ether-1, the primary reference fuel 90, and their blend: Experiments and modeling journal September 2022
Reaction Mechanism Generator: Automatic construction of chemical kinetic mechanisms journal June 2016
Improvement of emission characteristics and thermal efficiency in diesel engines by fueling gasoline/diesel/PODEn blends journal February 2016
Physico-chemical properties and fuel characteristics of oxymethylene dialkyl ethers journal June 2016
Homogeneous charge compression ignition (HCCI) combustion of polyoxymethylene dimethyl ethers (PODE) journal November 2016
Potentials to simplify the engine system using the alternative diesel fuels oxymethylene ether OME1 and OME3−6 on a heavy-duty engine journal January 2020
Auto-ignition of oxymethylene ethers (OMEn, n = 2–4) as promising synthetic e-fuels from renewable electricity: shock tube experiments and automatic mechanism generation journal March 2020
Experimental and numerical investigation of the Advanced Fuel Ignition Delay Analyzer (AFIDA) constant-volume combustion chamber as a research platform for fuel chemical kinetic mechanism validation journal April 2020
Chemical kinetic modeling of diethoxymethane oxidation: A carbon–neutral fuel journal May 2021
Property predictions demonstrate that structural diversity can improve the performance of polyoxymethylene ethers as potential bio-based diesel fuels journal July 2021
Effects of knock intensity measurement technique and fuel chemical composition on the research octane number (RON) of FACE gasolines: Part 1 – Lambda and knock characterization journal November 2021
Effect of fuel composition and EGR on spark-ignited engine combustion with LPG fueling: Experimental and numerical investigation journal November 2022
Using rapid compression machines for chemical kinetics studies journal October 2014
Knocking combustion in spark-ignition engines journal July 2017
Unravelling combustion mechanisms through a quantitative understanding of elementary reactions journal January 2005
Diethoxymethane as tailor-made fuel for gasoline controlled autoignition journal January 2019
Effects of injection strategies on combustion and emission characteristics of a common-rail diesel engine fueled with isopropanol-butanol-ethanol and diesel blends journal January 2019
A Comprehensive Experimental and Kinetic Modeling Study of the Combustion Chemistry of Diethoxymethane journal September 2021
Fuel Properties of Oxymethylene Ethers with Terminating Groups from Methyl to Butyl journal August 2022
Dimethoxymethane as a Cleaner Synthetic Fuel: Synthetic Methods, Catalysts, and Reaction Mechanism journal January 2019
Detailed Chemistry Promotes Understanding of Octane Numbers and Gasoline Sensitivity journal November 2006
A Shock Tube Study of n - and iso- Propanol Ignition journal December 2009
Trioxane as a Source of Formaldehyde journal August 1947
Density and Viscosity for Monoethanolamine + Water, + Ethanol, and + 2-Propanol journal January 1995
Density and Viscosity Measurements of 2,2,4-Trimethylpentane (Isooctane) from 198 K to 348 K and up to 100 MPa journal January 1996
One-pot 1,1-dimethoxymethane synthesis from methanol: a promising pathway over bifunctional catalysts journal January 2016
Computational kinetics of the hydrogen abstraction reactions of n -propanol and iso-propanol by OH radical journal January 2019
Calculation of Flame Ionization Detector Relative Response Factors Using the Effective Carbon Number Concept journal August 1985
Investigations on Spark and Corona Ignition of Oxymethylene Ether-1 and Dimethyl Carbonate Blends with Gasoline by High-Speed Evaluation of OH* Chemiluminescence journal March 2018