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Title: Effect of initial orientation on dynamic recrystallization of a zirconium alloy during hot deformation

Journal Article · · Materials Characterization
;  [1];  [2]; ;  [3]; ;  [1]
  1. College of Materials Science and Engineering, Chongqing University, Chongqing 400044 (China)
  2. National Engineering Research Center for Equipment and Technology of Cold Strip Rolling, College of Mechanical Engineering, Yanshan University, Qinhuangdao 066004 (China)
  3. State Key Laboratory of Metastable Materials Science and Technology, Yanshan University, Qinhuangdao 066004 (China)

Highlights: • The dynamic recrystallization process is enhanced by the operation of slip. • Continuous dynamic recrystallization is promoted by the rotation of grains. • Texture induced hardening hides the softening induced by dynamic recrystallization. - Abstract: The present study investigated the influence of the initial orientation on the dynamic recrystallization (DRX) behavior of a Zr-1Sn-0.3Nb alloy. A hot-rolled and annealed Zr sheet was compressed along two directions: along the normal direction so that the grains' -axis was nearly parallel to the loading direction (0° sample) and along the transverse direction so that the grains' -axis was nearly perpendicular to the loading direction (90° sample). The samples were compressed at 700 °C at a strain rate of 1 s{sup −1}. The microstructures at different strains were characterized by the electron backscatter diffraction (EBSD) technique, and conventional dislocation analysis using transmission electron microscope (TEM) was performed. A threshold value of grain orientation spread (GOS) equaled to 5° was used to distinguish the dynamically recrystallized grains from the deformed matrix. The results revealed that the DRX behavior strongly depended on the initial orientation. The Schmid factor analysis and TEM observation confirmed that pyramidal slip operated from the first stage of deformation in the 0° sample but not in the 90° sample. For the 0° sample, in the early and medium stages of deformation, due to the high stored energy caused by the operation of pyramidal slip, DDRX was mainly contributed to the formation of new fine grains. However, in the later stage of deformation, the DRX mechanism changed from DDRX to CDRX. In the 90° sample, although DDRX featured by grain boundary bulging occurred, the main DRX mechanism was CDRX in the whole deformation processing. Moreover, texture induced hardening in the early stage of deformation hides the softening induced by DDRX.

OSTI ID:
22805876
Journal Information:
Materials Characterization, Vol. 145; Other Information: Copyright (c) 2017 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA); ISSN 1044-5803
Country of Publication:
United States
Language:
English

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