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High-temperature damage evolution in 10 keV He+ irradiated W and W-5Re

Journal Article · · Materials Characterization
 [1];  [2];  [3]; ; ; ;  [1]
  1. School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083 (China)
  2. Department of Materials Science, Faculty of Science and Engineering, Shimane University, 1060 Nishikawatsu, Matsue 690-8504 (Japan)
  3. Department of Materials, University of Oxford, Parks Road, OX1 3PH Oxford (United Kingdom)

Highlights: • High-temperature damage in pure W appeared strongly dependent upon foil thickness. • Visible bubbles occurred at above a threshold fluence of ~ 4.5×10{sup 19} He{sup +}/m{sup 2}. • Dislocations with b = ½ were identified and exhibited a wavy morphology. • The bypass of bubbles by dislocations operated through simple shear. • Rhenium gave rise to ~ 10-40% increase in bubble size and a pronounced change in bubble morphology. - Abstract: High-temperature damage evolution in pure W and W-5Re has been studied by combining transmission electron microscopy and in-situ irradiations with 10 keV He{sup +} ions. The irradiations covered a temperature range of T{sub irr} = 773–1473 K and a fluence range of (4.5–15) × 10{sup 19} He{sup +}/m{sup 2}. In pure W, detailed characterizations have shown that damage evolution is highly dependent upon the foil thickness. Regions of thickness irr from 773 K to 1473 K, a pronounced bubble growth and an increased degree of bubble ordering were observed. In thicker regions (≳100 nm), 1/2<111> dislocation loops and line entanglements were found up to 1473 K, and were often seen to be decorated with helium bubbles. In W-5Re, areas of different foil thickness exhibited only small differences in damage evolution. The densities of bubbles were comparable to those seen in pure W at all temperatures, while the average size of bubbles was found to be ~10–40% higher. The damage microstructure transformed from a mixture of dislocation loops and bubbles at 773 K to dislocation line entanglements decorated with bubbles at 1473 K.

OSTI ID:
22805835
Journal Information:
Materials Characterization, Journal Name: Materials Characterization Vol. 145; ISSN 1044-5803; ISSN MACHEX
Country of Publication:
United States
Language:
English

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