Synthesis and Crystal Structure of a Chalcone Derivative

Journal Article · Thu Dec 14 23:00:00 EST 2017 · Crystallography Reports

DOI:https://doi.org/10.1134/S1063774517070240· OSTI ID:22758288

Singh, Vikram D. ^[1]; Salian, Vinutha V.; Narayana, B. ^[2]; Sarojini, B. K. ^[3]; Kamni, ^[1]; Anthal, Sumati; Kant, Rajni ^[4]

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1. Shri Mata Vaishno Devi University, School of Physics (India)
2. Mangalore University, Department of Studies in Chemistry (India)
3. Mangalore University, Department of Industrial Chemistry (India)
4. University of Jammu, X-ray Crystallography Laboratory, Post-Graduate Department of Physics and Electronics (India)

(2E)-3-(anthrance-9-yl)-1-(3,4-dichlorophenyl)prop-2-en-1-one [C{sub 23}H{sub 14}OC{sub l2}] is synthesized and its crystal structure is determined by single X-ray diffraction. There exist two molecules in the asymmetric unit. The dihedral angle between the benzene and anthracene moiety of the molecule A and B is 86.51(12)° and 76.42(13)°, respectively. No classical hydrogen bonds are observed and only van der Waals forces stabilize the crystal packing.

• OSTI ID: 22758288
• Journal Information: Crystallography Reports, Journal Name: Crystallography Reports Journal Issue: 7 Vol. 62; ISSN 1063-7745; ISSN CYSTE3
• Country of Publication: United States
• Language: English

Related Subjects

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
75 CONDENSED MATTER PHYSICS
SUPERCONDUCTIVITY AND SUPERFLUIDITY
ANTHRACENE
ASYMMETRY
BENZENE
CRYSTAL STRUCTURE
HYDROGEN
MOLECULES
SYNTHESIS
VAN DER WAALS FORCES
X-RAY DIFFRACTION