Synthesis, Characterization, Crystal Structure, and Hirshfeld Surface Analysis of Ethyl 2-(4-bromophenyl)-1-cyclohexyl-1H-benzo[d]imidazole-5-carboxylate
Journal Article
·
· Crystallography Reports
- Mangalore University, Department of Studies in Chemistry (India)
- Mangalore University, PURSE Laboratory (India)
- Mangalore University, Department of Materials Science (India)
The title compound, C{sub 22}H{sub 23}N{sub 2}BrO{sub 2} was synthesized via one-pot reductive cyclization method and characterized by CNH analysis, FT-IR, UV-visible, mass, {sup 1}H and {sup 13}C NMR spectra, thermogravimetric analysis (TGA) and single crystal X-ray diffraction method. The compound crystallizes in monoclinic crystal system: sp. gr. P2{sub 1}/c, Z = 4. The crystal data reveals that the intermolecular interactions of the C–H···π and π···π type connect the molecules which was also visualized with the help of Hirshfeld surface analysis.
- OSTI ID:
- 22758220
- Journal Information:
- Crystallography Reports, Vol. 63, Issue 4; Other Information: Copyright (c) 2018 Pleiades Publishing, Inc.; Country of input: International Atomic Energy Agency (IAEA); ISSN 1063-7745
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
75 CONDENSED MATTER PHYSICS
SUPERCONDUCTIVITY AND SUPERFLUIDITY
37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
CARBON 13
CYCLIZATION
DIFFRACTION METHODS
FOURIER TRANSFORM SPECTROMETERS
HYDROGEN 1
IMIDAZOLES
INFRARED SPECTRA
MOLECULES
MONOCLINIC LATTICES
MONOCRYSTALS
NUCLEAR MAGNETIC RESONANCE
SURFACES
SYNTHESIS
THERMAL GRAVIMETRIC ANALYSIS
ULTRAVIOLET SPECTRA
X-RAY DIFFRACTION
SUPERCONDUCTIVITY AND SUPERFLUIDITY
37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
CARBON 13
CYCLIZATION
DIFFRACTION METHODS
FOURIER TRANSFORM SPECTROMETERS
HYDROGEN 1
IMIDAZOLES
INFRARED SPECTRA
MOLECULES
MONOCLINIC LATTICES
MONOCRYSTALS
NUCLEAR MAGNETIC RESONANCE
SURFACES
SYNTHESIS
THERMAL GRAVIMETRIC ANALYSIS
ULTRAVIOLET SPECTRA
X-RAY DIFFRACTION