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Title: Local and transient nanoscale strain mapping during in situ deformation

Journal Article · · Applied Physics Letters
DOI:https://doi.org/10.1063/1.4961683· OSTI ID:22590482
 [1]; ;  [2];  [3]
  1. National Center for Electron Microscopy, Molecular Foundry, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States)
  2. Gatan, Inc., Pleasanton, California 94588 (United States)
  3. Hysitron, Inc., Minneapolis, Minnesota 55344 (United States)

The mobility of defects such as dislocations controls the mechanical properties of metals. This mobility is determined both by the characteristics of the defect and the material, as well as the local stress and strain applied to the defect. Therefore, the knowledge of the stress and strain during deformation at the scale of defects is important for understanding fundamental deformation mechanisms. Here, we demonstrate a method of measuring local stresses and strains during continuous in situ deformation with a resolution of a few nanometers using nanodiffraction strain mapping. Our results demonstrate how large multidimensional data sets captured with high speed electron detectors can be analyzed in multiple ways after an in situ TEM experiment, opening the door for true multimodal analysis from a single electron scattering experiment.

OSTI ID:
22590482
Journal Information:
Applied Physics Letters, Vol. 109, Issue 8; Other Information: (c) 2016 Author(s); Country of input: International Atomic Energy Agency (IAEA); ISSN 0003-6951
Country of Publication:
United States
Language:
English

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Cited By (7)

Variable‐Wavelength Quick Scanning Nanofocused X‐Ray Microscopy for In Situ Strain and Tilt Mapping journal January 2020
In Situ Transmission Electron Microscopy book January 2019
Manifold learning of four-dimensional scanning transmission electron microscopy journal January 2019
Local nanoscale strain mapping of a metallic glass during in situ testing journal April 2018
Advances in in situ nanomechanical testing journal June 2019
Insights into fundamental deformation processes from advanced in situ transmission electron microscopy journal June 2019
Recent Advances in Transmission Electron Microscopy for Materials Science at the EMAT Lab of the University of Antwerp journal July 2018