skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Preparation of cubic boron nitride films by RF bias sputtering

Conference ·
OSTI ID:223670

Cubic boron nitride (cBN) films were successfully prepared by the phase-regulated rf bias sputtering with the aid of magnetic field. The effects of the substrate bias voltage (V{sub s}), the working gas pressure (p) and the deposition time were investigated systematically. Cubic phase was formed in the filmed deposited with V{sub s} above the threshold which depended on p. Even at p = 0.4 mTorr, cBN films were grown with V{sub s} above 100 V. The prepared cBN films had a double-layered structure which consists of an initially deposited layer of sp{sup 2} phase and a layer of cubic phase subsequently grown. The maximum growth rate of the cubic layer was estimated to be approximately 1 nm/s. Stress measurements of the cBN films were also carried out, revealing that the cBN films had compressive stress of a few GPa.

Research Organization:
International Union of Pure and Applied Chemistry; American Physical Society, New York, NY (United States)
OSTI ID:
223670
Report Number(s):
CONF-950875-Vol.4; TRN: 96:002548-0005
Resource Relation:
Conference: 12. international symposium on plasma chemistry, Minneapolis, MN (United States), 21-25 Aug 1995; Other Information: PBD: Jul 1995; Related Information: Is Part Of 12th International symposium on plasma chemistry. Proceedings, Volume 4; Heberlein, J.V.; Ernie, D.W.; Roberts, E.D. [eds.] [Minnesota Univ., Minneapolis, MN (United States)]; PB: 615 p.
Country of Publication:
United States
Language:
English

Similar Records

The synthesis, characterization, and mechanical properties of thick, ultrahard cubic boron nitride films deposited by ion-assisted sputtering
Journal Article · Fri Aug 01 00:00:00 EDT 1997 · Journal of Applied Physics · OSTI ID:223670

Evidence for rhombohedral boron nitride in cubic boron nitride films grown by ion-assisted deposition
Journal Article · Thu Sep 15 00:00:00 EDT 1994 · Physical Review, B: Condensed Matter; (United States) · OSTI ID:223670

Low-temperature growth of low friction wear-resistant amorphous carbon nitride thin films by mid-frequency, high power impulse, and direct current magnetron sputtering
Journal Article · Tue Sep 15 00:00:00 EDT 2015 · Journal of Vacuum Science and Technology. A, Vacuum, Surfaces and Films · OSTI ID:223670