Electroextraction of boron from boron carbide scrap
- Chemistry Group, Indira Gandhi Centre for Atomic Research, Kalpakkam – 603102 (India)
- Physical Metallurgy Group, Indira Gandhi Centre for Atomic Research, Kalpakkam – 603102 (India)
- Materials Science Group, Indira Gandhi Centre for Atomic Research, Kalpakkam – 603102 (India)
Studies were carried out to extract elemental boron from boron carbide scrap. The physicochemical nature of boron obtained through this process was examined by characterizing its chemical purity, specific surface area, size distribution of particles and X-ray crystallite size. The microstructural characteristics of the extracted boron powder were analyzed by using scanning electron microscopy and transmission electron microscopy. Raman spectroscopic examination of boron powder was also carried out to determine its crystalline form. Oxygen and carbon were found to be the major impurities in boron. Boron powder of purity ∼ 92 wt. % could be produced by the electroextraction process developed in this study. Optimized method could be used for the recovery of enriched boron ({sup 10}B > 20 at. %) from boron carbide scrap generated during the production of boron carbide. - Highlights: • Recovery of {sup 10}B from nuclear grade boron carbide scrap • Development of process flow sheet • Physicochemical characterization of electroextracted boron • Microscopic examination of electroextracted boron.
- OSTI ID:
- 22288669
- Journal Information:
- Materials Characterization, Journal Name: Materials Characterization Vol. 84; ISSN 1044-5803; ISSN MACHEX
- Country of Publication:
- United States
- Language:
- English
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