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Structure of substituted 2-(phenoxy)benzimidazoles

Journal Article · · Crystallography Reports
 [1]; ; ;  [2];  [1]
  1. Ural State Forestry University (Russian Federation)
  2. Russian Academy of Sciences, Institute of Organic Synthesis, Ural Branch (Russian Federation)

The synthesis and X-ray diffraction study of 1-benzyl-2-[2-(5-ethyltetrazole-2-yl)-phenoxy]-1H-benzimidazole and 1-benzyl-2-[2-(5-ethyltetrazole-2-yl)-4-nitrophenoxy]-1H-benzimidazole single crystals have been performed. The oxidative splitting of an azo-hydrazone group of 1-(2-hydroxy-(5-nitro)phenyl)-3-ethyl-5-(benzylbenzimidazolyl)formazans, a break in the C2-N1 bond, the interaction of o-hydroxyl group of aryl fragment with oxygen, and the formation of new 2-(phenoxy)benzimidazoles are found to occur in the presence of perchlorate iron(III).

OSTI ID:
22156322
Journal Information:
Crystallography Reports, Journal Name: Crystallography Reports Journal Issue: 2 Vol. 58; ISSN 1063-7745; ISSN CYSTE3
Country of Publication:
United States
Language:
English