Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Thiol‐Functionalized Conjugated Metal–Organic Frameworks for Stable and Efficient Perovskite Photovoltaics

Journal Article · · Advanced Science
 [1];  [2];  [1];  [3];  [3];  [1];  [4];  [2];  [5];  [6];  [7];  [3];  [6]
  1. State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, School of Materials Science and Engineering Wuhan University of Technology Wuhan 430070 China, Hoffmann Institute of Advanced Materials Shenzhen Polytechnic 7098 Liuxian Boulevard Shenzhen 518055 China
  2. Molecular Foundry Division Lawrence Berkeley National Laboratory Berkeley CA 94720 USA
  3. The Hong Kong Polytechnic University Shenzhen Research Institute Guangdong Shenzhen 518057 China, Department of Electronic and Information Engineering, Research Institute for Smart Energy (RISE) The Hong Kong Polytechnic University Hung Hom Kowloon Hong Kong 999077 China
  4. Shenzhen Key Laboratory of Polymer Science and Technology, College of Materials Science and Engineering Shenzhen University Shenzhen 518060 China
  5. International Collaborative Laboratory of 2D Materials for Optoelectronics Science and Technology of Ministry of Education, Institute of Microscale Optoelectronics Shenzhen University Shenzhen 518060 China
  6. Hoffmann Institute of Advanced Materials Shenzhen Polytechnic 7098 Liuxian Boulevard Shenzhen 518055 China
  7. State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, School of Materials Science and Engineering Wuhan University of Technology Wuhan 430070 China
Abstract

Metal–organic frameworks (MOFs) have been investigated recently in perovskite photovoltaics owing to their potential to boost optoelectronic performance and device stability. However, the impact of variations in the MOF side chain on perovskite characteristics and the mechanism of MOF/perovskite film formation remains unclear. In this study, three nanoscale thiol‐functionalized UiO‐66‐type Zr‐based MOFs (UiO‐66‐(SH) 2 , UiO‐66‐MSA, and UiO‐66‐DMSA) are systematically employed and examined in perovskite solar cells (PSCs). Among these MOFs, UiO‐66‐(SH) 2 , with its rigid organic ligands, exhibited a strong interaction with perovskite materials with more efficient suppression of perovskite vacancy defects. More importantly, A detailed and in‐depth discussion is provided on the formation mechanism of UiO‐66‐(SH) 2 ‐assisted perovskite film upon in situ GIWAXS performed during the annealing process. The incorporation of UiO‐66‐(SH) 2 additives substantially facilitates the conversion of PbI 2 into the perovskite phase, prolongs the duration of stage I, and induces a delayed phase transformation pathway. Consequently, the UiO‐66‐(SH) 2 ‐assisted device demonstrates reduced defect density and superior optoelectronic properties with optimized power conversion efficiency of 24.09% and enhanced long‐term stability under ambient environment and continuous light illumination conditions. This study acts as a helpful design guide for desired MOF/perovskite structures, enabling further advancements in MOF/perovskite optoelectronic devices.

Research Organization:
Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)
Sponsoring Organization:
Guangdong Basic and Applied Basic Research Foundation; Hong Kong Polytechnic University; National Natural Science Foundation of China; Research Grants Council of Hong Kong; Shenzhen Science and Technology Innovation Commission; USDOE; USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division (MSE)
Grant/Contract Number:
AC02-05CH11231
OSTI ID:
2205400
Alternate ID(s):
OSTI ID: 2367191
OSTI ID: 2205402
Journal Information:
Advanced Science, Journal Name: Advanced Science Journal Issue: 4 Vol. 11; ISSN 2198-3844
Publisher:
Wiley Blackwell (John Wiley & Sons)Copyright Statement
Country of Publication:
Germany
Language:
English

References (39)

Manipulation of Perovskite Crystallization Kinetics via Lewis Base Additives journal January 2021
Two‐Dimensional Metal–Organic Frameworks‐Based Grain Termination Strategy Enables High‐Efficiency Perovskite Photovoltaics with Enhanced Moisture and Thermal Stability journal February 2021
Self‐Organized Small Molecules in Robust MOFs for High‐Performance Perovskite Solar Cells with Enhanced Degradation Activation Energy journal June 2022
Planar Heterojunction Perovskite Solar Cells Incorporating Metal-Organic Framework Nanocrystals journal October 2015
Phase Transition Control for High Performance Ruddlesden-Popper Perovskite Solar Cells journal April 2018
Manipulating the Mixed‐Perovskite Crystallization Pathway Unveiled by In Situ GIWAXS journal April 2019
Precise Control of Perovskite Crystallization Kinetics via Sequential A‐Site Doping journal September 2020
Perovskite Quantum Wells Formation Mechanism for Stable Efficient Perovskite Photovoltaics—A Real‐Time Phase‐Transition Study journal December 2020
Synergistic Effects of Eu‐MOF on Perovskite Solar Cells with Improved Stability journal August 2021
Ionic Liquid Control Crystal Growth to Enhance Planar Perovskite Solar Cells Efficiency journal July 2016
Efficient Defect Passivation for Perovskite Solar Cells by Controlling the Electron Density Distribution of Donor‐π‐Acceptor Molecules journal March 2019
A Two‐Dimensional Hole‐Transporting Material for High‐Performance Perovskite Solar Cells with 20 % Average Efficiency journal July 2018
Thermally Stable D2h Symmetric Donor‐π‐Donor Porphyrins as Hole‐Transporting Materials for Perovskite Solar Cells journal August 2022
Linker Vacancy Engineering of a Robust ftw‐type Zr‐MOF for Hexane Isomers Separation journal May 2023
Revealing Size‐Dependency of Ionic Liquid to Assist Perovskite Film Formation Mechanism for Efficient and Durable Perovskite Solar Cells journal May 2023
The Role of Ionic Liquids in Performance Enhancement of Two‐Step Perovskite Photovoltaics journal November 2022
Recent Progress in Ionic Liquids for Stability Engineering of Perovskite Solar Cells journal May 2022
Remarkable quality improvement of CsPbIBr2 perovskite film by cellulose acetate addition for efficient and stable carbon-based inorganic perovskite solar cells journal November 2021
Metal-organic framework nanocrystals enabled efficient and durable two-step perovskite photovoltaics journal March 2023
MOF-derived ZnO as electron transport layer for improving light harvesting and electron extraction efficiency in perovskite solar cells journal January 2020
Metal-organic frameworks with mixed-ligands strategy as heterogeneous nucleation center to assist crystallization for efficient and stable perovskite solar cells journal February 2023
Multifunctional nanostructured host-guest POM@MOF with lead sequestration capability induced stable and efficient perovskite solar cells journal June 2022
Advance and prospect of metal-organic frameworks for perovskite photovoltaic devices journal July 2022
Elucidating the Failure Mechanisms of Perovskite Solar Cells in Humid Environments Using In Situ Grazing-Incidence Wide-Angle X-ray Scattering journal August 2018
Tuning Metal–Organic Framework (MOF) Topology by Regulating Ligand and Secondary Building Unit (SBU) Geometry: Structures Built on 8-Connected M6 (M = Zr, Y) Clusters and a Flexible Tetracarboxylate for Propane-Selective Propane/Propylene Separation journal November 2022
Topologically guided tuning of Zr-MOF pore structures for highly selective separation of C6 alkane isomers journal May 2018
Out-of-equilibrium processes in crystallization of organic-inorganic perovskites during spin coating journal September 2021
Mapping structure heterogeneities and visualizing moisture degradation of perovskite films with nano-focus WAXS journal November 2022
Stabilization of 3D/2D perovskite heterostructures via inhibition of ion diffusion by cross-linked polymers for solar cells with improved performance journal February 2023
2D/3D heterojunction engineering at the buried interface towards high-performance inverted methylammonium-free perovskite solar cells journal July 2023
2D metal–organic framework for stable perovskite solar cells with minimized lead leakage journal September 2020
Engineering the buried interface in perovskite solar cells via lattice-matched electron transport layer journal July 2023
Perovskite solar cells based on screen-printed thin films journal November 2022
High-yield, green and scalable methods for producing MOF-303 for water harvesting from desert air journal October 2022
An autonomous wearable biosensor powered by a perovskite solar cell journal July 2023
The first depleted heterojunction TiO2–MOF-based solar cell journal January 2014
Hybrid origin of a primate, the gray snub-nosed monkey journal June 2023
Inactive (PbI 2 ) 2 RbCl stabilizes perovskite films for efficient solar cells journal July 2022
The Crystal Orbital Hamilton Population (COHP) Method as a Tool to Visualize and Analyze Chemical Bonding in Intermetallic Compounds journal May 2018