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Synthesis and structure of (Rb{sub 0.50}Ba{sub 0.25})[UO{sub 2}(CH{sub 3}COO){sub 3}]

Journal Article · · Crystallography Reports
;  [1];  [2]
  1. Russian Academy of Sciences, Institute of Inorganic Chemistry, Siberian Branch (Russian Federation)
  2. Samara State University (Russian Federation)
A new compound (Rb{sub 0.50}Ba{sub 0.25})[UO{sub 2}(CH{sub 3}COO){sub 3}] is synthesized and its crystal structure is studied by X-ray diffraction. The compound crystallizes in the form of yellow plates belonging to the cubic crystal system. The unit cell parameter a = 17.0367(1) A, V = 4944.89(5) A{sup 3}, space group I 4 bar 3d, Z = 16, and R = 0.0182. The coordination polyhedron of the uranium atom is a hexagonal bipyramid with oxygen atoms of three acetate groups and the uranyl group in the vertices. The crystal chemical formula of the uranium-containing group is AB{sub 3}{sup 01}(A = UO{sub 2}{sup 2+}, B{sup 01} = CH{sub 3}COO{sup -}). The oxygen atoms of the acetate groups that enter the coordination polyhedron of uranium are bound to barium and rubidium atoms.
OSTI ID:
22051227
Journal Information:
Crystallography Reports, Journal Name: Crystallography Reports Journal Issue: 2 Vol. 55; ISSN 1063-7745; ISSN CYSTE3
Country of Publication:
United States
Language:
English