Submicrometer Single Crystal Diffractometry for Highly Accurate Structure Determination

Journal Article · Wed Jun 23 00:00:00 EDT 2010 · AIP Conference Proceedings

DOI:https://doi.org/10.1063/1.3463161· OSTI ID:21410217

Yasuda, Nobuhiro; Fukuyama, Yoshimitsu; Kimura, Shigeru ^[1]; Toriumi, Koshiro ^[2]; Takata, Masaki ^[1]

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1. Japan Synchrotron Radiation Research Institute, 1-1-1 Kouto, Sayo, Sayo, Hyogo 679-5198 (Japan)
2. Japan Science and Technology Agency, CREST, 5, Sanbancho, Chiyoda, Tokyo 102-0075 (Japan)

Submicrometer single crystal diffractometry for highly accurate structure determination was developed using the extremely stable and highly brilliant synchrotron radiation from SPring-8. This was achieved using a microbeam focusing system and the submicrometer precision low-eccentric goniometer system. We demonstrated the structure analyses with 2x2x2 {mu}m{sup 3} cytidine, 600x600x300 nm{sup 3} BaTiO{sub 3}, and 1x1x1 {mu}m{sup 3} silicon. The observed structure factors of the silicon crystal were in agreement with the structure factors determined by the Pendelloesung method and do not require absorption and extinction corrections.

• OSTI ID: 21410217
• Journal Information: AIP Conference Proceedings, Vol. 1234, Issue 1; Conference: SRI 2009: 10. international conference on radiation instrumentation, Melbourne (Australia), 27 Sep - 2 Oct 2009; Other Information: DOI: 10.1063/1.3463161; (c) 2010 American Institute of Physics; ISSN 0094-243X
• Country of Publication: United States
• Language: English

Related Subjects

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY
ABSORPTION
ACCURACY
BARIUM COMPOUNDS
CORRECTIONS
CYTIDINE
DIFFRACTOMETERS
GONIOMETERS
MONOCRYSTALS
OPTICS
PLATES
SILICON
SPRING-8 STORAGE RING
STRUCTURE FACTORS
SYNCHROTRON RADIATION
TITANATES
X RADIATION
ALKALINE EARTH METAL COMPOUNDS
AZINES
BREMSSTRAHLUNG
CRYSTALS
DIMENSIONLESS NUMBERS
ELECTROMAGNETIC RADIATION
ELEMENTS
HETEROCYCLIC COMPOUNDS
IONIZING RADIATIONS
MEASURING INSTRUMENTS
NUCLEOSIDES
NUCLEOTIDES
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
OXYGEN COMPOUNDS
PYRIMIDINES
RADIATION SOURCES
RADIATIONS
RIBOSIDES
SEMIMETALS
SORPTION
STORAGE RINGS
SYNCHROTRON RADIATION SOURCES
TITANIUM COMPOUNDS
TRANSITION ELEMENT COMPOUNDS