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Title: Ag{sub 2}S morphology controllable via simple template-free solution route

Journal Article · · Materials Research Bulletin
 [1]
  1. Key Laboratory of Rare Earth Chemistry and Physics, Changchun Institute of Applied Chemistry, Graduate School of the Chinese Academy of Sciences, Chinese Academy of Sciences, Changchun 130022 (China)

Different morphologies of Ag{sub 2}S nano- and micro-materials, including spokewise micrometer bars, microfibers, nanowires, worm-like nanoparticles and nanopolyhedrons have been obtained controllably by a facile one-step method at room temperature. Powder X-ray diffraction (XRD), X-ray photo-electron spectroscopy (XPS) and scanning electron microscope (SEM) were employed to characterize the structure and compositions of those nanomaterials. Furthermore, ultraviolet visible (UV-vis) spectra of Ag{sub 2}S with different morphologies show different spectral features. In this route, no any organic template materials were added into the reaction container. The concentrations of ammonia, Ag{sup +}, S{sup 2-} and their ratios in the solution may play an important role on the morphologies and sizes of the products.

OSTI ID:
21144097
Journal Information:
Materials Research Bulletin, Vol. 43, Issue 8-9; Other Information: DOI: 10.1016/j.materresbull.2007.08.004; PII: S0025-5408(07)00362-5; Copyright (c) 2007 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved; Country of input: International Atomic Energy Agency (IAEA); ISSN 0025-5408
Country of Publication:
United States
Language:
English