High-Throughput Structure/Function Screening of Materials and Catalysts with Multiple Spectroscopic Techniques

Journal Article · Fri Feb 02 00:00:00 EST 2007 · AIP Conference Proceedings

DOI:https://doi.org/10.1063/1.2644684· OSTI ID:21054762

Tromp, Moniek; Russu, Sergio; Russell, Andrea E; Guerin, Sam; Hayden, Brian E; Suchsland, Jens-Peter; Frey, Jeremy G; Binsted, Norman ^[1]; Dent, Andy J; Mosselmans, J Fred W. ^[2]; Harvey, Ian; Hayama, Shu; Fiddy, Steven ^[3]; Meacham, Ken; Surridge, Michael ^[4]; Tsapatsaris, Nikolaos; Beesley, Angela M; Schroeder, Sven L. M. ^[5]; Newton, Mark A; Safonova, Olga V ^[6]

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1. University of Southampton, School of Chemistry, Southampton, SO17 1BJ (United Kingdom)
2. Diamond Light Source, Chilton, OX11 0DE (United Kingdom)
3. CCRLC, SRS Daresbury Laboratory, Daresbury (United Kingdom)
4. IT Innovation Centre, Chilworth Science Park, Southampton, SO16 7NP (United Kingdom)
5. University of Manchester, Manchester (United Kingdom)
6. ESRF, Grenoble (France)

High throughput screening methodologies are expanded to synchrotron based x-ray absorption techniques. An environmental chamber, based on ultra-high vacuum equipment, has been developed allowing in situ studies on arrays of samples while X-ray absorption fine structure spectroscopy, Raman spectroscopy, mass spectrometry and/or X-ray diffraction can be applied simultaneously to characterize the system under process conditions in a time-resolved manner. The chamber accommodates a diverse range of samples from surface science to materials chemistry to heterogeneous catalysis. Data acquisition and data logging software is developed to handle large quantities of divers but related information. New data logging, processing and analysis procedures and programs are developed which will allow fast structure-function relationships characterization.

• OSTI ID: 21054762
• Journal Information: AIP Conference Proceedings, Vol. 882, Issue 1; Conference: XAFS13: 13. international conference on X-ray absorption fine structure, Stanford, CA (United States), 9-14 Jul 2006; Other Information: DOI: 10.1063/1.2644684; (c) 2007 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA); ISSN 0094-243X
• Country of Publication: United States
• Language: English

Related Subjects

37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
ABSORPTION SPECTRA
ABSORPTION SPECTROSCOPY
CATALYSTS
DATA ACQUISITION
FINE STRUCTURE
HETEROGENEOUS CATALYSIS
MASS SPECTROSCOPY
RAMAN SPECTROSCOPY
STRUCTURE FUNCTIONS
SURFACES
TIME RESOLUTION
X-RAY DIFFRACTION
X-RAY SPECTRA
X-RAY SPECTROSCOPY