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The effect of microstructural evolution on hardening behavior of type 17-4PH stainless steel in long-term aging at 350 deg. C

Journal Article · · Materials Characterization
 [1];  [2];  [2];  [2];  [3]
  1. School of Materials Science and Engineering, Sichuan University, Chengdu, 610065 (China) and Nuclear Power Institute of China, Chengdu, 610041 (China)
  2. Nuclear Power Institute of China, Chengdu, 610041 (China)
  3. School of Materials Science and Engineering, Sichuan University, Chengdu, 610065 (China)

The effect of microstructural evolution on hardening behavior of 17-4PH stainless steel in long-term aging at 350 deg. C was studied by X-ray diffraction and transmission electron microscopy. The results showed that there is the matrix of lath martensite and nanometer-sized particles of {epsilon}-Cu precipitated from the matrix after the alloy is solution treated and tempered. When the alloy was aged 350 deg. C for 9 months, {alpha}-{alpha}' spinodal decomposition occurred along the grain boundaries and caused an increase in hardness which compensated for the weakening effect due to ripening of the {epsilon}-copper precipitates. Upon further aging to 12 months, the Cr-rich {alpha}'-phase and M{sub 23}C{sub 6} precipitated, both of which strengthened the alloy considerably and led to enhanced hardening despite the continued softening by overaging of the {epsilon}-copper precipitates. With the aging time extended to 15 months, substantial reversed austenite transformed and precipitation of the intermetallic G-phase occurred near the {epsilon}-Cu precipitates in the matrix. The abundant amount of reversed austenite that transformed led to rapid softening.

OSTI ID:
20889853
Journal Information:
Materials Characterization, Journal Name: Materials Characterization Journal Issue: 4-5 Vol. 57; ISSN 1044-5803; ISSN MACHEX
Country of Publication:
United States
Language:
English

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