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Title: Geopolymeric materials prepared using Class F fly ash and elevated temperature curing

Journal Article · · Cement and Concrete Research
 [1]
  1. Department of Civil Engineering, Monash University, Clayton, Victoria 3800 (Australia)

This paper reports the results of the study of the influence of elevated temperature curing on phase composition, microstructure and strength development in geopolymer materials prepared using Class F fly ash and sodium silicate and sodium hydroxide solutions. In particular, the effect of storage at room temperature before the application of heat on strength development and phase composition was studied. X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and SEM were utilised in this study. Long precuring at room temperature before application of heat was beneficial for strength development in all studied materials, as strength comparable to 1 month of curing at elevated temperature can develop in this case only after 24 h of heat curing. The main product of reaction in the geopolymeric materials was amorphous alkali aluminosilicate gel. However, in the case of sodium hydroxide activator in addition to it, traces of chabazite, Linde Type A, Na-P1 (gismondine) zeolites and hydroxysodalite were also present. The type of zeolite present and composition of aluminosilicate gel were dependent on the curing history.

OSTI ID:
20706220
Journal Information:
Cement and Concrete Research, Vol. 35, Issue 6; Other Information: DOI: 10.1016/j.cemconres.2004.06.031; PII: S0008-8846(04)00284-4; Copyright (c) 2004 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved; Country of input: International Atomic Energy Agency (IAEA); ISSN 0008-8846
Country of Publication:
United States
Language:
English