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Luminescence decay kinetics of Mn{sup 2+}-doped ZnS nanoclusters grown in reverse micelles

Journal Article · · Physical Review. B, Condensed Matter and Materials Physics
 [1];  [1];  [2];  [2]
  1. Department of Chemistry, University of California, Santa Cruz, California 95060 (United States)
  2. Pacific Northwest National Laboratory (PNNL), P.O. Box 999, Richland, Washington 99352 (United States)
We report the synthesis and luminescence decay kinetics of 1.2-nm Mn{sup 2+}-doped ZnS nanoclusters grown in reverse micelles. The preparation method produces small particles with narrow-size distribution and fluorescence bands near 400-450 nm and 585 nm. Time-dependent fluorescence decay measurements using picosecond, nanosecond, and millisecond techniques reveal relaxation processes on all three time scales. In the doped sample, the red emission detected at 600 nm exhibits a 1-2 ms decay in addition to faster decays with time constants on the order of hundreds of ps, a few ns and tens of {mu}s. While the slow decay is the same as that of bulk Mn{sup 2+}-doped ZnS, the fast decays are present for both doped and undoped samples and are unique to nanocluster ZnS, which are attributed to deep trap-state emission. The blue luminescence near 400-450 nm is attributed to shallow trap-state emission of ZnS. These results help to resolve the controversy in the literature regarding the lifetime of the Mn{sup 2+} emission in Mn-doped ZnS nanoparticles. (c) 2000 The American Physical Society.
OSTI ID:
20217120
Journal Information:
Physical Review. B, Condensed Matter and Materials Physics, Journal Name: Physical Review. B, Condensed Matter and Materials Physics Journal Issue: 3 Vol. 62; ISSN 1098-0121
Country of Publication:
United States
Language:
English

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