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Title: Interplay of strain and phase evolution of laser powder bed fusion Ti–6Al–4V

Journal Article · · Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing
ORCiD logo [1];  [2];  [2];  [3];  [4];  [2];  [1]
  1. Johns Hopkins Univ., Baltimore, MD (United States)
  2. Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
  3. Drexel Univ., Philadelphia, PA (United States)
  4. Exponent Engineering and Science Consulting, Philadelphia, PA (United States)

While additive manufacturing (AM) provides a method of producing geometrically complex and highly detailed structures, the generation of residual strain in AM processes like laser powder bed fusion (L-PBF) can negatively impact performance-enabling properties. In applications such as orthopedic implants, specific performance windows require optimized microstructures in order to obtain desirable properties from multi-phase alloys like Ti–6Al–4V. This research aims to quantify the microscale origins of strain in L-PBF manufactured Ti–6Al–4V by understanding how strain is distributed at the grain and sub-grain scale, the interplay between phase evolution and strain, and examining post-processing strain relief strategies to control these features. Model spinal cage implants were manufactured from Ti–6Al–4V powder via L-PBF and then subjected to strain relieving heat treatment cycles above and below the Ti–6Al–4V β transus as a function of time and cooling rate. Residual strain was then studied via high resolution electron backscatter diffraction (HR-EBSD), and 2D strain maps with sub-micron resolution were generated for each post-processing state. It was found that macroscale thermal strains decreased with heat treatment time, but additional contributions from phase stabilizing residual strains retained primarily in the α' grains as lattice distortive strain remained. Additionally, the retention of β phase significantly changed the strain and dislocation distribution while reducing overall residual strain. In conclusion, these results were validated and reinforced with 3D mesoscopic micromechanical modeling of strain behavior across simulated microstructures, confirming that the local lattice dilation of α’ martensite is a primary contributor of microscale strain generation and retention in L-PBF Ti–6Al–4V.

Research Organization:
Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA); US Department of the Navy, Office of Naval Research (ONR); USDOE Laboratory Directed Research and Development (LDRD) Program
Grant/Contract Number:
AC52-07NA27344; B646330; N00014-20-1-2788; 18-SI-003
OSTI ID:
2007598
Alternate ID(s):
OSTI ID: 1890541
Report Number(s):
LLNL-JRNL-823443; 1036177
Journal Information:
Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing, Vol. 855; ISSN 0921-5093
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English

References (48)

A Spectral Iterative Method for the Computation of Effective Properties Of Elastically Inhomogeneous Polycrystals journal March 2012
Titanium: The implant material of today journal November 1987
Energy and emissions saving potential of additive manufacturing: the case of lightweight aircraft components journal November 2016
Residual stresses in selective laser sintering and selective laser melting journal October 2006
Fatigue characterization of Titanium Ti-6Al-4V samples produced by Additive Manufacturing journal January 2016
Identifying strain localization and dislocation processes in fatigued Inconel 718 manufactured from selective laser melting journal May 2018
Microstructural control in metal laser powder bed fusion additive manufacturing using laser beam shaping strategy journal February 2020
A study of the microstructural evolution during selective laser melting of Ti–6Al–4V journal May 2010
Effect of Stress Relieving Heat Treatment on the Microstructure and High-Temperature Compressive Deformation Behavior of Ti-6Al-4V Alloy Manufactured by Selective Laser Melting journal August 2018
Role of Processing in Microstructural Evolution in Inconel 625: A Comparison of Three Additive Manufacturing Techniques journal April 2021
Heat treatment of Ti6Al4V produced by Selective Laser Melting: Microstructure and mechanical properties journal November 2012
High resolution surface morphology measurements using EBSD cross-correlation techniques and AFM journal July 2011
Multiscale Characterization of Microstructure and Residual Strain Distribution in Additively Manufactured Inconel 625 journal August 2019
Ductility improvement due to martensite α′ decomposition in porous Ti–6Al–4V parts produced by selective laser melting for orthopedic implants journal February 2016
Microstructure Evolution, Tensile Properties, and Fatigue Damage Mechanisms in Ti-6Al-4V Alloys Fabricated by Two Additive Manufacturing Techniques journal January 2015
Phase-field modeling of displacive phase transformations in elastically anisotropic and inhomogeneous polycrystals journal September 2014
Early Stages of Microstructure and Texture Evolution during Beta Annealing of Ti-6Al-4V journal December 2017
Martensite Formation and Decomposition during Traditional and AM Processing of Two-Phase Titanium Alloys—An Overview journal March 2021
Selective laser melting of biocompatible metals for rapid manufacturing of medical parts journal August 2007
Fatigue performance evaluation of selective laser melted Ti–6Al–4V journal March 2014
Metal additive-manufacturing process and residual stress modeling journal February 2016
Subsurface Cooling Rates and Microstructural Response during Laser Based Metal Additive Manufacturing journal February 2020
Fatigue Behaviour of Additively Manufactured Ti-6Al-4V journal January 2015
Texture Analysis with MTEX – Free and Open Source Software Toolbox journal February 2010
Accuracy assessment of elastic strain measurement by EBSD journal February 2009
Strains, planes, and EBSD in materials science journal September 2012
Variant selection during α precipitation in Ti–6Al–4V under the influence of local stress – A simulation study journal September 2013
Direct metal laser sintering of TI6Al4V alloy for patient-specific temporo mandibular joint prosthesis and implant journal January 2021
Evolution of lattice strain in Ti–6Al–4V during tensile loading at room temperature journal December 2008
Fully porous 3D printed titanium femoral stem to reduce stress-shielding following total hip arthroplasty journal October 2016
Geometrically necessary dislocations and strain gradient plasticity––a dislocation dynamics point of view journal January 2003
Effect of heat treatment on the tensile behavior of selective laser melted Ti-6Al-4V by in situ X-ray characterization journal May 2020
Role of martensite decomposition in tensile properties of selective laser melted Ti-6Al-4V journal May 2018
Effects of heat treatments on microstructure and properties of Ti-6Al-4V ELI alloy fabricated by electron beam melting (EBM) journal February 2017
On the Localization of Plastic Strain in Microtextured Regions of Ti-6Al-4V journal February 2021
Additive manufacturing of Ti6Al4V alloy: A review journal February 2019
Titanium in Biomedical Applications—Properties and Fabrication: A Review journal August 2015
Material Incress Manufacturing by Rapid Prototyping Techniques journal January 1991
Precise measurement of strain accommodation in austenite matrix surrounding martensite in ferrous alloys by electron backscatter diffraction analysis journal February 2009
A phase-field model of stress effect on grain boundary migration journal March 2011
A Further Analysis on Ti6Al4V Lattice Structures Manufactured by Selective Laser Melting journal September 2019
Selective laser melting of Al–8.5Fe–1.3V–1.7Si alloy: Investigation on the resultant microstructure and hardness journal April 2015
Strain hardening of Titanium alloy Ti6Al4V sheets with prior heat treatment and cold working journal April 2016
Comparison of nanoscale measurements of strain and stress using electron back scattered diffraction and confocal Raman microscopy journal November 2008
Dissolution of the Alpha Phase in Ti-6Al-4V During Isothermal and Continuous Heat Treatment journal March 2019
Microstructural and mechanical approaches of the selective laser melting process applied to a nickel-base superalloy journal February 2012
Perspectives on Titanium Science and Technology journal February 2013
On the mechanical behaviour of titanium alloy TiAl6V4 manufactured by selective laser melting: Fatigue resistance and crack growth performance journal March 2013