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Divergent Stabilities of Tetravalent Cerium, Uranium, and Neptunium Imidophosphorane Complexes**

Journal Article · · Angewandte Chemie
 [1];  [1];  [2];  [1];  [1];  [2];  [3]
  1. School of Chemistry and Biochemistry Georgia Institute of Technology Atlanta GA 30332-0400 USA
  2. Department of Chemistry The University of Akron Akron OH 44325-3601 USA
  3. School of Chemistry and Biochemistry Georgia Institute of Technology Atlanta GA 30332-0400 USA, Nuclear and Radiological Engineering Program Georgia Institute of Technology Atlanta GA 30332-0400 USA

Abstract

The study of the redox chemistry of mid‐actinides (U−Pu) has historically relied on cerium as a model, due to the accessibility of trivalent and tetravalent oxidation states for these ions. Recently, dramatic shifts of lanthanide 4+/3+ non‐aqueous redox couples have been established within a homoleptic imidophosphorane ligand framework. Herein we extend the chemistry of the imidophosphorane ligand (NPC=[N=P t Bu(pyrr) 2 ] ; pyrr=pyrrolidinyl) to tetrahomoleptic NPC complexes of neptunium and cerium ( 1‐M , 2‐M , M=Np, Ce) and present comparative structural, electrochemical, and theoretical studies of these complexes. Large cathodic shifts in the M 4+/3+ (M=Ce, U, Np) couples underpin the stabilization of higher metal oxidation states owing to the strongly donating nature of the NPC ligands, providing access to the U 5+/4+ , U 6+/5+ , and to an unprecedented, well‐behaved Np 5+/4+ redox couple. The differences in the chemical redox properties of the U vs . Ce and Np complexes are rationalized based on their redox potentials, degree of structural rearrangement upon reduction/oxidation, relative molecular orbital energies, and orbital composition analyses employing density functional theory.

Sponsoring Organization:
USDOE
Grant/Contract Number:
SC0019385
OSTI ID:
1994887
Journal Information:
Angewandte Chemie, Journal Name: Angewandte Chemie Journal Issue: 34 Vol. 135; ISSN 0044-8249
Publisher:
Wiley Blackwell (John Wiley & Sons)Copyright Statement
Country of Publication:
Germany
Language:
English

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