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Hydrogen Stability and Bonding in SiNx and Al2O3 Dielectric Stacks on Poly-Si/SiOx Passivating Contacts

Journal Article · · ACS Applied Energy Materials
 [1];  [2];  [2];  [1];  [1]
  1. Colorado School of Mines, Golden, CO (United States); National Renewable Energy Laboratory (NREL), Golden, CO (United States)
  2. National Renewable Energy Laboratory (NREL), Golden, CO (United States)

Polycrystalline Si on SiOx passivating contacts enables some of the highest efficiency single-junction Si photovoltaic devices, but the high-temperature firing process needed for industrial metallization can significantly reduce passivation. We show that after firing, the implied open-circuit voltage, iVoc, for the Al2O3/SiNx/poly-Si/SiOx/c-Si stack is 20-30 mV higher than the SiNx/Al2O3/poly-Si/SiOx/c-Si stack and therefore provides better passivation of the SiOx/c-Si interface. Using effusion measurements and Fourier transform infrared spectroscopy, we demonstrate that more than twice as much hydrogen is retained in the dielectric up to the peak firing temperature of ~800 degrees C for Al2O3-capped structures. If the Al2O3 layer is not present in the stack, after firing, the iVoc is lower by 50-100 mV compared to Al2O3/SiNx or SiNx/Al2O3 stacks. These studies will inform future work on the role of dielectrics in aiding the passivation of poly-Si/SiOx passivating contacts.

Research Organization:
National Renewable Energy Laboratory (NREL), Golden, CO (United States)
Sponsoring Organization:
USDOE Office of Energy Efficiency and Renewable Energy (EERE), Renewable Power Office. Solar Energy Technologies Office
Grant/Contract Number:
AC36-08GO28308
OSTI ID:
1993046
Report Number(s):
NREL/JA-5900-85901; MainId:86674; UUID:fa6dafd2-d1ad-4989-a333-18c3d4eb6727; MainAdminID:69796
Journal Information:
ACS Applied Energy Materials, Journal Name: ACS Applied Energy Materials Journal Issue: 13 Vol. 6; ISSN 2574-0962
Publisher:
American Chemical Society (ACS)Copyright Statement
Country of Publication:
United States
Language:
English

References (66)

Surface passivation of crystalline silicon solar cells: a review journal January 2000
Design, fabrication and characterisation of a 24.4% efficient interdigitated back contact solar cell: 24.4% efficient interdigitated back contact solar cell journal October 2014
Firing stability of tube furnace‐annealed n‐type poly‐Si on oxide junctions
  • Hollemann, Christina; Rienäcker, Michael; Soeriyadi, Anastasia
  • Progress in Photovoltaics: Research and Applications, Vol. 30, Issue 1 https://doi.org/10.1002/pip.3459
journal August 2021
Silicon Nitride Encapsulated Silicon Nanocrystals for Lithium Ion Batteries journal December 2015
Dielectric surface passivation for silicon solar cells: A review journal June 2017
The role of hydrogenation and gettering in enhancing the efficiency of next‐generation Si solar cells: An industrial perspective journal June 2017
Annealing behavior of hydrogenated amorphous silicon—nitrogen alloy films prepared by sputtering journal October 1983
Impact of the firing temperature profile on light induced degradation of multicrystalline silicon journal October 2016
Atomic‐Layer‐Deposited Al 2 O 3 as Effective Barrier against the Diffusion of Hydrogen from SiN x :H Layers into Crystalline Silicon during Rapid Thermal Annealing journal October 2020
Hydrogenation Mechanisms of Poly‐Si/SiO x Passivating Contacts by Different Capping Layers journal November 2019
Characteristic Study of Silicon Nitride Films Deposited by LPCVD and PECVD journal April 2018
The formation of hydrogen permeation barriers on steels by aluminising journal May 1991
Tritium permeation barriers for fusion technology journal March 1995
Influence of microstructure on the hydrogen permeation of alumina coatings journal July 2013
Study of the composition of hydrogenated silicon nitride SiNx:H for efficient surface and bulk passivation of silicon journal August 2009
Efficient carrier-selective p- and n-contacts for Si solar cells journal December 2014
The application of poly-Si/SiOx contacts as passivated top/rear contacts in Si solar cells journal January 2017
Impact of hydrogen on the boron-oxygen-related lifetime degradation and regeneration kinetics in crystalline silicon journal October 2021
Origins of silicon solar cell passivation by SiNx:H anneal journal April 2002
Alumina sputtered on MANET as an effective deuterium permeation barrier journal November 1998
Hot-wire chemical vapor deposition of high hydrogen content silicon nitride for solar cell passivation and anti-reflection coating applications journal April 2003
Low-Temperature Conformal Atomic Layer Deposition of SiNx Films Using Si2Cl6 and NH3 Plasma journal May 2015
Chemical Passivation of Crystalline Si by Al2O3 Deposited Using Atomic Layer Deposition: Implications for Solar Cells journal June 2021
Dehydrogenation Reactions during Atomic Layer Deposition of Ru Using O2 journal September 2012
A Deuterium Labeling, FTIR, and Ab Initio Investigation of the Solution-Phase Thermal Reactions of Alcohols and Alkenes with Hydrogen-Terminated Silicon Surfaces journal June 2000
A passivating contact for silicon solar cells formed during a single firing thermal annealing journal September 2018
Separating the two polarities of the POLO contacts of an 26.1%-efficient IBC solar cell journal January 2020
Atomic structure of light-induced efficiency-degrading defects in boron-doped Czochralski silicon solar cells journal January 2021
Passivation and depassivation of silicon dangling bonds at the Si/SiO 2 interface by atomic hydrogen journal September 1993
Detailed study of the composition of hydrogenated SiNx layers for high-quality silicon surface passivation journal September 2002
Fourier transform infrared spectroscopy of annealed silicon-rich silicon nitride thin films journal November 2008
The hydrogen content of plasma-deposited silicon nitride journal April 1978
Hydrogen bonding configurations in silicon nitride films prepared by plasma‐enhanced deposition journal July 1985
Annealing of plasma silicon oxynitride films journal October 1986
Hydrogen induced passivation of Si interfaces by Al2O3 films and SiO2/Al2O3 stacks journal October 2010
Thermal dissociation process of hydrogen atoms in plasma-enhanced chemical vapor deposited silicon nitride films journal November 1998
Influence of annealing and Al2O3 properties on the hydrogen-induced passivation of the Si/SiO2 interface journal May 2012
Absolute partial cross sections for electron-impact ionization of H2O and D2O from threshold to 1000 eV journal January 1998
Carrier-selective contacts for Si solar cells journal May 2014
High-temperature degradation in plasma-enhanced chemical vapor deposition Al 2 O 3 surface passivation layers on crystalline silicon journal August 2014
Tunnel oxide passivated contacts formed by ion implantation for applications in silicon solar cells journal November 2015
Composition limited hydrogen effusion rate of a-SiNx:H passivation stack
  • Jafari, Sahar; Hirsch, Jens; Lausch, Dominik
  • 15th International Conference on Concentrator Photovoltaic Systems (CPV-15), AIP Conference Proceedings https://doi.org/10.1063/1.5123853
conference January 2019
Connection between Si–N and Si–H vibrational properties in amorphous SiNx: H films journal March 1989
Structural interpretation of the vibrational spectra of a -Si: H alloys journal February 1979
Local atomic structure in thin films of silicon nitride and silicon diimide produced by remote plasma-enhanced chemical-vapor deposition journal May 1986
Configurational statistics in a - Si x N y H z alloys: A quantitative bonding analysis journal October 1988
Free-energy model for bonding in amorphous covalent alloys journal February 1991
Dynamic behavior of hydrogen in silicon nitride and oxynitride films made by low-pressure chemical vapor deposition journal August 1993
Thermal effusion measurements: Probing hydrogen in surface passivation schemes conference June 2012
Firing Stability of Polysilicon Passivating Contacts: The Role of Hydrogen conference June 2021
Analysis of Silicon Solar Cells With Poly-Si/SiOx Carrier-Selective Base and Emitter Contacts journal January 2018
Carrier-Induced Degradation in Multicrystalline Silicon: Dependence on the Silicon Nitride Passivation Layer and Hydrogen Released During Firing journal March 2018
Controlling Light- and Elevated-Temperature-Induced Degradation With Thin Film Barrier Layers journal January 2020
Understanding Light- and Elevated Temperature-Induced Degradation in Silicon Wafers Using Hydrogen Effusion Mass Spectroscopy journal November 2021
Passivation Enhancement of Poly-Si Carrier-Selective Contacts by Applying ALD Al2O3 Capping Layers journal January 2022
Hydrogen Permeability of Sintered Aluminum Oxide journal September 1979
Hydrogen Permeation Measurements on Alumina: Hydrogen Permeation Measurements on Alumina journal December 2004
Dissociation reactions of hydrogen in remote plasma-enhanced chemical-vapor-deposition silicon nitride journal September 2001
Measurement of absolute radical densities in a plasma using modulated-beam line-of-sight threshold ionization mass spectrometry
  • Agarwal, Sumit; Quax, Guido W. W.; van de Sanden, M. C. M.
  • Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films, Vol. 22, Issue 1 https://doi.org/10.1116/1.1627767
journal January 2004
Deposition of silicon dioxide and silicon nitride by remote plasma enhanced chemical vapor deposition
  • Lucovsky, G.; Richard, P. D.; Tsu, D. V.
  • Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films, Vol. 4, Issue 3 https://doi.org/10.1116/1.573832
journal May 1986
Investigations of N-H and Si-N Bonding Configurations in Hydrogenated Amorphous Silicon Nitride Films by Infrared Absorption Spectroscopy journal November 1985
Properties of Plasma-Deposited Silicon Nitride journal January 1979
Passivation and Depassivation of Si–SiO[sub 2] Interfaces with Atomic Hydrogen journal January 2009
Review—Investigation and Review of the Thermal, Mechanical, Electrical, Optical, and Structural Properties of Atomic Layer Deposited High- k Dielectrics: Beryllium Oxide, Aluminum Oxide, Hafnium Oxide, and Aluminum Nitride journal January 2017
Polycrystalline silicon passivated tunneling contacts for high efficiency silicon solar cells journal March 2016
Microstructure Characterization of Amorphous Silicon-Nitride Films by Effusion Measurements journal January 2006

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