In-situ synchrotron X-ray diffraction investigation on deformation behavior of Nb/NiTi composite during pre-straining process

Guo, Shun; Zhang, Hui-hui; Kwak, Min-kyung; Ding, Wang; Liu, Guang-lei; Ma, Wen; Liu, Hai-xia; Meng, Qing-kun; Zhao, Xin-qing

doi:10.1016/s1003-6326(22)65970-3

Title: In-situ synchrotron X-ray diffraction investigation on deformation behavior of Nb/NiTi composite during pre-straining process

Journal Article · Thu Sep 15 00:00:00 EDT 2022 · Transactions of the Nonferrous Metals Society of China

DOI:https://doi.org/10.1016/s1003-6326(22)65970-3· OSTI ID:1981801

Guo, Shun ^[1]; Zhang, Hui-hui ^[1]; Kwak, Min-kyung ^[2]; Ding, Wang ^[1]; Liu, Guang-lei ^[1]; Ma, Wen ^[3]; Liu, Hai-xia ^[1]; Meng, Qing-kun ^[4]; Zhao, Xin-qing ^[5]

Jiangnan University, Zhenjiang (China)
Seoul National University (Korea, Republic of)
Jiangnan University, Zhenjiang (China); Youke Publishing Co., Ltd., Beijing (China)
China University of Mining and Technology, Xuzhou, Jiangsu (China)
Beihang University, Beijing (China)

The mechanisms responsible for deformation behavior in Nb/NiTi composite during pre-straining were investigated systematically using in-situ synchrotron X-ray diffraction, transmission electron microscopy and tensile test. It is shown that upon loading, the composite experiences elastic elongation and slight plastic deformation of B19', B2 and β-Nb phases, together with the forward stress-induced martensitic (SIM) transformation from B2 to B19'. Upon unloading, the deformation mechanisms of the composite mainly involve elastic recovery of B19', B2 and β-Nb phases, compression deformation of β-Nb phase and incomplete B19'→B2 reverse SIM transformation. In the tensile loading-unloading procedure, besides the inherent elastic deformation and SIM transformation, the (001) compound twins in B19' martensite can also be conducive to the elastic deformation occurring in B19'-phase of the composite. Therefore, this composite can exhibit a large recoverable strain after unloading owing to the elastic deformation, and the partially reversible and consecutive SIM transformation together with the (001) compound twins.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); National Natural Science Foundation of China (NSFC); Six Talent Peaks Project in Jiangsu Province; Zhenjiang Science & Technology Program; Jiangsu University

Grant/Contract Number:: AC02-06CH11357; 51771082; 51971009; 52175410; 51801076; 2019-XCL-113; GY2020001; NZXB20200101

OSTI ID:: 1981801

Journal Information:: Transactions of the Nonferrous Metals Society of China, Vol. 32, Issue 8; ISSN 1003-6326

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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36 MATERIALS SCIENCE
Nb/NiTi composite
near-linear deformation behavior
large recoverable strain
martensitic transformation

Title: In-situ synchrotron X-ray diffraction investigation on deformation behavior of Nb/NiTi composite during pre-straining process

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