Thickness-dependent phase transition kinetics in lithium-intercalated MoS2

Pondick, Joshua V.; Yazdani, Sajad; Kumar, Aakash; Hynek, David J.; Hart, James L.; Wang, Mengjing; Qiu, Diana Y.; Cha, Judy J.

doi:10.1088/2053-1583/ac4e9b

Thickness-dependent phase transition kinetics in lithium-intercalated MoS₂

Journal Article · Thu Feb 03 23:00:00 EST 2022 · 2D Materials

DOI:https://doi.org/10.1088/2053-1583/ac4e9b· OSTI ID:1979456

^[1]; Yazdani, Sajad ^[2]; ^[2]; ^[2]; ^[2]; ^[2]; ^[2]; ^[2]

Yale Univ., New Haven, CT (United States); OSTI
Yale Univ., New Haven, CT (United States)

The phase transitions of two-dimensional (2D) materials are key to the operation of many devices with applications including energy storage and low power electronics. Nanoscale confinement in the form of reduced thickness can modulate the phase transitions of 2D materials both in their thermodynamics and kinetics. Here, using in situ Raman spectroscopy we demonstrate that reducing the thickness of MoS₂ below five layers slows the kinetics of the phase transition from 2H- to 1T'-MoS₂ induced by the electrochemical intercalation of lithium. In this study, we observe that the growth rate of 1T' domains is suppressed in thin MoS₂ supported by SiO₂, and attribute this growth suppression to increased interfacial effects as the thickness is reduced below 5 nm. In this study, the suppressed kinetics can be reversed by placing MoS₂ on a 2D hexagonal boron nitride (hBN) support, which readily facilitates the release of strain induced by the phase transition. Additionally, we show that the irreversible conversion of intercalated 1T'-MoS₂ into Li2S and Mo is also thickness-dependent and the stability of 1T'-MoS₂ is significantly increased below five layers, requiring a much higher applied electrochemical potential to break down 1T'-MoS₂ into Li₂S and Mo nanoclusters.

View Accepted Manuscript (DOE)

Research Organization:: Yale Univ., New Haven, CT (United States); Univ. of California, Oakland, CA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF)

Grant/Contract Number:: SC0021965; AC02-05CH11231

OSTI ID:: 1979456

Journal Information:: 2D Materials, Journal Name: 2D Materials Journal Issue: 2 Vol. 9; ISSN 2053-1583

Publisher:: IOP PublishingCopyright Statement

Country of Publication:: United States

Language:: English

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