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Title: A real time sorbent based air monitoring system for determining low level airborne exposure levels to Lewisite

Book ·
OSTI ID:197424
 [1];  [2];  [3]
  1. Army Edgewood Research, Development and Engineering Center, Aberdeen Proving Ground, MD (United States). Chemical Support Div.
  2. Dynatherm Analytical Instruments, Inc., Kelton, PA (United States)
  3. SciTech Services, Inc., Abingdon, MD (United States)

The Real Time Analytical Platform (RTAP) is designed to provide mobile, real-time monitoring support to ensure protection of worker safety in areas where military unique compounds are used and stored, and at disposal sites. Quantitative analysis of low-level vapor concentrations in air is accomplished through sorbent-based collection with subsequent thermal desorption into a gas chromatograph (GC) equipped with a variety of detectors. The monitoring system is characterized by its sensitivity (ability to measure at low concentrations), selectivity (ability to filter out interferences), dynamic range and linearity, real time mode (versus methods requiring extensive sample preparation procedures), and ability to interface with complimentary GC detectors. This presentation describes an RTAP analytical method for analyzing lewisite, an arsenical compound, that consists of a GC screening technique with an Electron Capture Detector (ECD), and a confirmation technique using an Atomic Emission Detector (AED). Included in the presentation is a description of quality assurance objectives in the monitoring system, and an assessment of method accuracy, precision and detection levels.

OSTI ID:
197424
Report Number(s):
CONF-9405167-; TRN: IM9612%%198
Resource Relation:
Conference: Measurement of toxic and related air pollutants, Durham, NC (United States), 3-6 May 1994; Other Information: PBD: 1994; Related Information: Is Part Of Measurement of toxic and related air pollutants. Proceedings of the 1994 U.S. EPA/A and WMA international symposium; PB: 1075 p.
Country of Publication:
United States
Language:
English