skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Novel ΔE-ΔE-E Diamond Detector Development (Final Report)

Technical Report ·
OSTI ID:1902974
 [1]
  1. Great Lakes Crystal Technologies, East Lansing, MI (United States)

Nuclear physics research has a growing need for high performance devices to detect, analyze, and track photons, charged particles, and neutral particles such as neutrons, neutrinos, and single atoms. Accurately detecting the position, time, and rate of particles as they strike in high flux radiation environments like those in the Facility for Rare Isotope Beams (FRIB) is paramount to the success of current and future nuclear physics experiments. Much work has been performed with silicon and germanium to increase the detector efficiency and radiation hardness. However, their relatively narrow bandgaps present performance limitations and due to the relative ease with which silicon and germanium atoms can be displaced in their crystal lattice their ultimate lifetime is limited. New solid state detector technologies based on wide and ultra-wide bandgap semiconductor materials are of great interest. This purpose of the project is to develop novel monolithic diamond detector technology with multiple ΔE segments to measure the full energy loss curve versus depth of heavy ion penetration. The structure is a diamond detector formed by multiple layers of intrinsic detector grade diamond and thin layers of p+ electrically conducting diamond. Each p+/intrinsic/p+ layer set forms its own detector layer for measuring the energy deposited across the thickness of the intrinsic section. The design allows the intrinsic layer thicknesses to be either (1) the same or (2) a gradient of thicknesses versus depth of the heavy ion penetration. The ability to arbitrarily pick the number of detector layers and the thickness of each layer allows designs for specific nuclear physics applications. Phase I developed and tested initial devices and learned about design improvements. In Phase II improved devices will be developed and then tested at FRIB for sensing heavy ions. In Phase I, GLCT developed a heavily boron doped CVD growth process, and synthesized two samples, one for practice and the second as the deliverable sample. The deliverable sample was processed into a device using metallization. Assessment of the electrical properties of the device layers showed that two of the three detector layers behaved as expected but the third detector layer showed signs of unintentional doping. As a result, we successfully produced a third sample that demonstrates our capability of synthesizing high purity, insulating diamond on top of heavily boron doped diamond. Testing of the device revealed that our current device fabrication capabilities result in unallowably high background noise. These results demonstrate our ability to produce this technology and inform the best approach to device fabrication in Phase II. Success in the proposed effort will lead to improved detector technologies for use at FRIB and other leading high energy research laboratories worldwide. This in turn will accelerate the progress of nuclear physics research which has since its early days provided incredible payoffs to society, including advances in cancer therapy, diagnostic instrumentation, homeland security monitoring, industrial power transmission, biomedicine and drug development, understanding turbulence for industrial applications, advanced protein analysis, and much more.

Research Organization:
Great Lakes Crystal Technologies, East Lansing, MI (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
SC0022404
OSTI ID:
1902974
Type / Phase:
SBIR (Phase I)
Report Number(s):
DOE-GLCT-0022404
Country of Publication:
United States
Language:
English