X-ray diffraction measurements and pressure determination in nanosecond compression of solids up to 600 GPa

Coppari, F.; Fratanduono, D. E.; Millot, M.; Kraus, R. G.; Lazicki, A.; Rygg, J. R.; Smith, R. F.; Eggert, J. H.

doi:10.1103/physrevb.106.134105

Title: X-ray diffraction measurements and pressure determination in nanosecond compression of solids up to 600 GPa

Journal Article · Fri Oct 14 00:00:00 EDT 2022 · Physical Review. B

DOI:https://doi.org/10.1103/physrevb.106.134105· OSTI ID:1901512

^[1];

^[1]; Lazicki, A. ^[1];

^[2]; Smith, R. F. ^[1]; Eggert, J. H. ^[1]

Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
Univ. of Rochester, NY (United States)

X-ray diffraction measurements under laser-driven dynamic compression now allow us to investigate the atomic structure of matter at TPa pressures and thousands of degree temperatures with broad implications for condensed matter physics, planetary science and astronomy. Furthermore, pressure determination in these experiments often relies on velocimetry measurements coupled with modeling that requires accurate knowledge of the optical and thermo-mechanical properties of a window material, resulting in significant systematic uncertainty. Here we demonstrate different approach applicable to X-ray diffraction experiments under quasi-isentropic ramp-compression based on the use of in-situ pressure calibrants, similar to the methods often adopted in static-compression experiments with diamond anvil cells. Focusing on experiments using a diamond window, we discuss challenges and mitigation strategies for the novel approach. Our study, in addition to providing new structural information of 5 metals up to hundreds of GPa, provides validation to the currently used methods based on time-resolved measurement of the diamond free-surface velocity, and reveals that the use of in-situ calibrants enables a factor of four reduction in the pressure uncertainty in these experiments.

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Research Organization:: Univ. of Rochester, NY (United States); Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: NA0003856; AC52-07NA27344

OSTI ID:: 1901512

Alternate ID(s):: OSTI ID: 2006754

Report Number(s):: LLNL-JRNL-828639; 2022-476; 1769; 2735; TRN: US2311087

Journal Information:: Physical Review. B, Vol. 106, Issue 13; ISSN 2469-9950

Publisher:: American Physical Society (APS)Copyright Statement

Country of Publication:: United States

Language:: English

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Title: X-ray diffraction measurements and pressure determination in nanosecond compression of solids up to 600 GPa

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