Energy dispersive x-ray diffraction of luminescent powders: A complement to visible phosphor thermometry

Hansen, L. E.; Westphal, E. R.; Kastengren, A. L.; Winters, C.

doi:10.1063/5.0101649

Energy dispersive x-ray diffraction of luminescent powders: A complement to visible phosphor thermometry

Journal Article · Tue Aug 09 00:00:00 EDT 2022 · Journal of Applied Physics

DOI:https://doi.org/10.1063/5.0101649· OSTI ID:1882607

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Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Purdue Univ., West Lafayette, IN (United States)
Argonne National Lab. (ANL), Lemont, IL (United States). Advanced Photon Source (APS)

Energy-dispersive x-ray diffraction of thermographic phosphors has been explored as a complementary temperature diagnostic to visible phosphor thermometry in environments where the temperature-dependent optical luminescence of the phosphors is occluded. Powder phosphor samples were heated from ambient to 300°C in incremental steps and probed with polychromatic synchrotron x rays; scattered photons were collected at a fixed diffraction angle of 3.9°. Crystal structure, lattice parameters, and coefficients of thermal expansion were calculated from the diffraction data. Finally, of the several phosphors surveyed, YAG:Dy, ZnO:Ga, and GOS:Tb were found to be excellent candidates for diffraction thermometry due to their strong, distinct diffraction peaks that shift in a repeatable and linear manner with temperature.

View Accepted Manuscript (DOE)

Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS); Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States)

Sponsoring Organization:: National Aeronautic and Space Administration (NASA); USDOE; USDOE Laboratory Directed Research and Development (LDRD) Program; USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC); USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division

Grant/Contract Number:: AC02-06CH11357; NA0003525

OSTI ID:: 1882607

Alternate ID(s):: OSTI ID: 1880379
OSTI ID: 1969124

Report Number(s):: SAND2022-10025J; 708566

Journal Information:: Journal of Applied Physics, Journal Name: Journal of Applied Physics Journal Issue: 6 Vol. 132; ISSN 0021-8979

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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47 OTHER INSTRUMENTATION
crystal structure
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synchrotrons
temperature metrology
thermal effects
thermal instruments
x-ray fluorescence

Energy dispersive x-ray diffraction of luminescent powders: A complement to visible phosphor thermometry

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