Laser Powder Bed Fusion of ODS 14YWT from Gas Atomization Reaction Synthesis Precursor Powders

Saptarshi, Sourabh; deJong, Matthew; Rock, Christopher; Anderson, Iver; Napolitano, Ralph; Forrester, Jennifer; Lapidus, Saul; Kaoumi, Djamel; Horn, Timothy

doi:10.1007/s11837-022-05418-6

Laser Powder Bed Fusion of ODS 14YWT from Gas Atomization Reaction Synthesis Precursor Powders

Journal Article · Tue Aug 02 00:00:00 EDT 2022 · JOM. Journal of the Minerals, Metals & Materials Society

DOI:https://doi.org/10.1007/s11837-022-05418-6· OSTI ID:1879550

Saptarshi, Sourabh; deJong, Matthew; Rock, Christopher; Anderson, Iver; Napolitano, Ralph; Forrester, Jennifer; Lapidus, Saul; Kaoumi, Djamel;

Abstract

Laser powder bed fusion (LPBF) additive manufacturing (AM) is a promising route for the fabrication of oxide dispersion strengthened (ODS) steels. In this study, 14YWT ferritic steel powders were produced by gas atomization reaction synthesis (GARS). The rapid solidification resulted in the formation of stable, Y-containing intermetallic Y ₂ Fe ₁₇ on the interior of the powder and a stable Cr-rich oxide surface. The GARS powders were consolidated with LPBF. Process parameter maps identified a stable process window resulting in a relative density of 99.8%. Transmission electron microscopy and high-energy x-ray diffraction demonstrated that during LPBF, the stable phases in the powder dissociated in the liquid melt pool and reacted to form a high density (1.7 × 10 ²⁰ /m ³ ) of homogeneously distributed Ti ₂ Y ₂ O ₇ pyrochlore dispersoids ranging from 17 to 57 nm. The use of GARS powder bypasses the mechanical alloying step typically required to produce ODS feedstock. Preliminary mechanical tests demonstrated an ultimate tensile and yield strength of 474 MPa and 312 MPa, respectively.

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Research Organization:: Ames Laboratory (AMES), Ames, IA (United States); Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Organization:: National Science Foundation (NSF); USDOE Advanced Research Projects Agency - Energy (ARPA-E); USDOE Office of Fossil Energy (FE); USDOE Office of Fossil Energy and Carbon Management (FECM); USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-06CH11357; AC02-07CH11358; AR0001379

OSTI ID:: 1879550

Alternate ID(s):: OSTI ID: 1881902
OSTI ID: 2248009

Report Number(s):: IS-J-10,864; PII: 5418

Journal Information:: JOM. Journal of the Minerals, Metals & Materials Society, Journal Name: JOM. Journal of the Minerals, Metals & Materials Society Journal Issue: 9 Vol. 74; ISSN 1047-4838

Publisher:: Springer Science + Business MediaCopyright Statement

Country of Publication:: United States

Language:: English

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Laser Powder Bed Fusion of ODS 14YWT from Gas Atomization Reaction Synthesis Precursor Powders

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