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Low-Z FIB Grids for Reducing Spurious Fluorescence and X-ray Overlaps

Journal Article · · Microscopy Today
 [1];  [2];  [3];  [3]
  1. EXpressLO LLC, Lehigh Acres, FL (United States)
  2. Alcorix Company, Plainfield, IL (United States)
  3. Sandia National Lab. (SNL-CA), Livermore, CA (United States)
Low-Z nanocrystalline diamond (NCD) grids have been developed to reduce spurious fluorescence and avoid X-ray peak overlaps or interferences between the specimen and conventional metal grids. Here, the low-Z NCD grids are non-toxic and safe to handle, conductive, can be subjected to high-temperature heating experiments, and may be used for analytical work in lieu of metal grids. Both a half-grid geometry, which can be used for any lift-out method, or a full-grid geometry that can be used for ex situ lift-out or thin film analyses, can be fabricated and used for experiments.
Research Organization:
Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA)
Grant/Contract Number:
NA0003525
OSTI ID:
1855806
Report Number(s):
SAND2022-2600J; 703917
Journal Information:
Microscopy Today, Journal Name: Microscopy Today Journal Issue: 2 Vol. 30; ISSN 1551-9295
Publisher:
Cambridge University PressCopyright Statement
Country of Publication:
United States
Language:
English

References (2)

Transmission Electron Microscopy book January 2009
Introduction to Focused Ion Beams book January 2005

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