A tungsten external heater for BX90 diamond anvil cells with a range up to 1700 K

Yan, J.; Doran, A.; MacDowell, A. A.; Kalkan, B.

doi:10.1063/5.0009663

A tungsten external heater for BX90 diamond anvil cells with a range up to 1700 K

Journal Article · Mon Jan 25 00:00:00 EST 2021 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/5.0009663· OSTI ID:1838427

^[1]; ^[2]; MacDowell, A. A. ^[2]; Kalkan, B. ^[1]

Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Univ. of California, Santa Cruz, CA (United States)
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)

Resistive heating of a sample in a diamond anvil cell (DAC) can generate a homogeneous temperature field across the sample chamber with reliable temperatures measured by a thermocouple. It is of importance in experiments aiming at exploring phase diagrams and quantifying thermoelastic properties of materials. Here, we present a ring-heater design developed for BX90 diamond anvil cells (DACs). Furthermore, it is made of a ring-shaped aluminum oxide holder hosting a tungsten wire coil inside and coupled with Ar + 2% H₂ gas to prevent oxidation during experiment. This modular plug-and-play design enables in situ studies of samples via x-ray diffraction up to a temperature of 1700 K. Temperature in the BX90 sample volume as measured through a thermocouple was calibrated using the melting point of gold. As an application of this design, we report the thermal expansion coefficient of MgO at 9.5(1) GPa.

View Accepted Manuscript (DOE)

Research Organization:: Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC02-05CH11231

OSTI ID:: 1838427

Alternate ID(s):: OSTI ID: 1762515

Journal Information:: Review of Scientific Instruments, Journal Name: Review of Scientific Instruments Journal Issue: 1 Vol. 92; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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A tungsten external heater for BX90 diamond anvil cells with a range up to 1700 K

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