Highly Crystalline Multimetallic Nanoframes with Three-Dimensional Electrocatalytic Surfaces

Chen, Chen; Kang, Yijin; Huo, Ziyang; Zhu, Zhongwei; Huang, Wenyu; Xin, Huolin L.; Snyder, Joshua D.; Li, Dongguo; Herron, Jeffrey A.; Mavrikakis, Manos; Chi, Miaofang; More, Karren L.; Li, Yadong; Markovic, Nenad M.; Somorjai, Gabor A.; Yang, Peidong; Stamenkovic, Vojislav R.

doi:10.1126/science.1249061

Title: Highly Crystalline Multimetallic Nanoframes with Three-Dimensional Electrocatalytic Surfaces

Journal Article · Thu Feb 27 00:00:00 EST 2014 · Science

DOI:https://doi.org/10.1126/science.1249061· OSTI ID:1833358

Chen, Chen ^[1]; Kang, Yijin ^[2]; Huo, Ziyang ^[3]; Zhu, Zhongwei ^[3]; Huang, Wenyu ^[3]; Xin, Huolin L. ^[4]; Snyder, Joshua D. ^[2]; Li, Dongguo ^[2]; Herron, Jeffrey A. ^[5]; Mavrikakis, Manos ^[5]; Chi, Miaofang ^[6]; More, Karren L. ^[7]; Li, Yadong ^[8]; Markovic, Nenad M. ^[2]; Somorjai, Gabor A. ^[3]; Yang, Peidong ^[9]; Stamenkovic, Vojislav R. ^[2]

Univ. of California, Berkeley, CA (United States). Dept. of Chemistry; Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Materials Science Division; Tsinghua Univ., Beijing (China). Dept. of Chemistry
Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division
Univ. of California, Berkeley, CA (United States). Dept. of Chemistry; Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Materials Science Division
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Materials Science Division
Univ. of Wisconsin, Madison, WI (United States). Dept. of Chemical and Biological Engineering
Division of Materials Science and Technology, Oak Ridge National Laboratory, Oak Ridge, TN 37831, USA.
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science & Technology Division
Tsinghua Univ., Beijing (China). Dept. of Chemistry
Univ. of California, Berkeley, CA (United States). Dept. of Chemistry; Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Materials Science Division; King Abdulaziz Univ., Jeddah (Saudi Arabia). Dept. of Chemistry; Univ. of California, Berkeley and Lawrence Berkeley National Lab. (LBNL), CA (United States). Kavli Energy NanoSciences Inst.

Control of structure at the atomic level can precisely and effectively tune catalytic properties of materials, enabling enhancement in both activity and durability. We synthesized a highly active and durable class of electrocatalysts by exploiting the structural evolution of platinum-nickel (Pt-Ni) bimetallic nanocrystals. The starting material, crystalline PtNi₃ polyhedra, transforms in solution by interior erosion into Pt₃Ni nanoframes with surfaces that offer three-dimensional molecular accessibility. The edges of the Pt-rich PtNi₃ polyhedra are maintained in the final Pt₃Ni nanoframes. Both the interior and exterior catalytic surfaces of this open-framework structure are composed of the nanosegregated Pt-skin structure, which exhibits enhanced oxygen reduction reaction (ORR) activity. The Pt₃Ni nanoframe catalysts achieved a factor of 36 enhancement in mass activity and a factor of 22 enhancement in specific activity, respectively, for this reaction (relative to state-of-the-art platinum-carbon catalysts) during prolonged exposure to reaction conditions.

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Research Organization:: Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States); Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division; USDOE Office of Energy Efficiency and Renewable Energy (EERE), Transportation Office. Fuel Cell Technologies Office; USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-06CH11357; AC02-05CH11231; FG02-05ER15731

OSTI ID:: 1833358

Alternate ID(s):: OSTI ID: 1357584

Journal Information:: Science, Vol. 343, Issue 6177; ISSN 0036-8075

Publisher:: AAASCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 2151 works

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Nanostructure Optimization of Platinum-Based Nanomaterials for Catalytic Applications Duan, Sibin; Du, Zhe; Fan, Hongsheng Nanomaterials, Vol. 8, Issue 11 https://doi.org/10.3390/nano8110949	journal	November 2018
Direct Spectroscopy for Probing the Critical Role of Partial Covalency in Oxygen Reduction Reaction for Cobalt-Manganese Spinel Oxides Long, Xinghui; Yu, Pengfei; Zhang, Nian Nanomaterials, Vol. 9, Issue 4 https://doi.org/10.3390/nano9040577	journal	April 2019

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