Solution-Phase Synthesis of Cesium Lead Halide Perovskite Nanowires

Zhang, Dandan; Eaton, Samuel W.; Yu, Yi; Dou, Letian; Yang, Peidong

doi:10.1021/jacs.5b05404

Title: Solution-Phase Synthesis of Cesium Lead Halide Perovskite Nanowires

Journal Article · Thu Jul 16 00:00:00 EDT 2015 · Journal of the American Chemical Society

DOI:https://doi.org/10.1021/jacs.5b05404· OSTI ID:1832456

Zhang, Dandan ^[1]; Eaton, Samuel W. ^[2]; Yu, Yi ^[2]; Dou, Letian ^[1]; Yang, Peidong ^[1]

Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Univ. of California, Berkeley, CA (United States)
Univ. of California, Berkeley, CA (United States)

Halide perovskites have attracted much attention over the past 5 years as a promising class of materials for optoelectronic applications. However, compared to hybrid organic-inorganic perovskites, the study of their pure inorganic counterparts, like cesium lead halides (CsPbX₃), lags far behind. Here, a catalyst-free, solution-phase synthesis of CsPbX₃ nanowires (NWs) is reported. These NWs are single-crystalline, with uniform growth direction, and crystallize in the orthorhombic phase. Both CsPbBr₃ and CsPbI₃ are photoluminescence active, with composition-dependent temperature and self-trapping behavior. These NWs with a well-defined morphology could serve as an ideal platform for the investigation of fundamental properties and the development of future applications in nanoscale optoelectronic devices based on all-inorganic perovskites.

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Research Organization:: Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-05CH11231

OSTI ID:: 1832456

Journal Information:: Journal of the American Chemical Society, Vol. 137, Issue 29; ISSN 0002-7863

Publisher:: American Chemical Society (ACS)Copyright Statement

Country of Publication:: United States

Language:: English

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Materials Discovery of Stable and Nontoxic Halide Perovskite Materials for High-Efficiency Solar Cells Jacobs, Ryan; Luo, Guangfu; Morgan, Dane arXiv https://doi.org/10.48550/arxiv.1904.05690	text	January 2019
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Shape-Pure, Nearly Monodispersed CsPbBr ₃ Nanocubes Prepared Using Secondary Aliphatic Amines Imran, Muhammad; Ijaz, Palvasha; Baranov, Dmitry Nano Letters, Vol. 18, Issue 12 https://doi.org/10.1021/acs.nanolett.8b03598	journal	November 2018
All-Inorganic Metal Halide Perovskite Nanocrystals: Opportunities and Challenges Zhang, Qiao; Yin, Yadong ACS Central Science, Vol. 4, Issue 6 https://doi.org/10.1021/acscentsci.8b00201	journal	May 2018
Doped Halide Perovskite Nanocrystals for Reabsorption-Free Luminescent Solar Concentrators Meinardi, Francesco; Akkerman, Quinten A.; Bruni, Francesco ACS Energy Letters, Vol. 2, Issue 10 https://doi.org/10.1021/acsenergylett.7b00701	journal	September 2017
Postsynthesis Transformation of Insulating Cs ₄ PbBr ₆ Nanocrystals into Bright Perovskite CsPbBr ₃ through Physical and Chemical Extraction of CsBr Palazon, Francisco; Urso, Carmine; De Trizio, Luca ACS Energy Letters, Vol. 2, Issue 10 https://doi.org/10.1021/acsenergylett.7b00842	journal	September 2017
Rationalizing and Controlling the Surface Structure and Electronic Passivation of Cesium Lead Halide Nanocrystals Bodnarchuk, Maryna I.; Boehme, Simon C.; ten Brinck, Stephanie ACS Energy Letters, Vol. 4, Issue 1 https://doi.org/10.1021/acsenergylett.8b01669	journal	November 2018
Strong Carrier–Phonon Coupling in Lead Halide Perovskite Nanocrystals Iaru, Claudiu M.; Geuchies, Jaco J.; Koenraad, Paul M. ACS Nano, Vol. 11, Issue 11 https://doi.org/10.1021/acsnano.7b05033	journal	September 2017
Exploration of Near-Infrared-Emissive Colloidal Multinary Lead Halide Perovskite Nanocrystals Using an Automated Microfluidic Platform Lignos, Ioannis; Morad, Viktoriia; Shynkarenko, Yevhen ACS Nano, Vol. 12, Issue 6 https://doi.org/10.1021/acsnano.8b01122	journal	May 2018
Crystal Structure, Morphology, and Surface Termination of Cyan-Emissive, Six-Monolayers-Thick CsPbBr ₃ Nanoplatelets from X-ray Total Scattering Bertolotti, Federica; Nedelcu, Georgian; Vivani, Anna ACS Nano, Vol. 13, Issue 12 https://doi.org/10.1021/acsnano.9b07626	journal	November 2019
Green Photoluminescence of Perovskite CsPb(Br_1–xI_x)₃ Nanocrystals for Wide Color Gamut Displays Miyata, Simpei; Iso, Yoshiki; Isobe, Tetsuhiko ACS Omega, Vol. 4, Issue 12 https://doi.org/10.1021/acsomega.9b01858	journal	September 2019
Nitrate Ion-Incorporated Stable Perovskite Nanocrystals by a Solvent-Free Mechanochemical Reaction Nim, Gaurav Kumar; Bansal, Parul; Kar, Prasenjit ACS Omega, Vol. 4, Issue 13 https://doi.org/10.1021/acsomega.9b02183	journal	September 2019
Colloidal Synthesis of Quantum Confined Single Crystal CsPbBr ₃ Nanosheets with Lateral Size Control up to the Micrometer Range Shamsi, Javad; Dang, Zhiya; Bianchini, Paolo Journal of the American Chemical Society, Vol. 138, Issue 23 https://doi.org/10.1021/jacs.6b03166	journal	June 2016
Highly Emissive Divalent-Ion-Doped Colloidal CsPb _{1– x} M _x Br ₃ Perovskite Nanocrystals through Cation Exchange van der Stam, Ward; Geuchies, Jaco J.; Altantzis, Thomas Journal of the American Chemical Society, Vol. 139, Issue 11 https://doi.org/10.1021/jacs.6b13079	journal	March 2017
Writing on Nanocrystals: Patterning Colloidal Inorganic Nanocrystal Films through Irradiation-Induced Chemical Transformations of Surface Ligands Palazon, Francisco; Prato, Mirko; Manna, Liberato Journal of the American Chemical Society, Vol. 139, Issue 38 https://doi.org/10.1021/jacs.7b05888	journal	August 2017
Large lattice distortions and size-dependent bandgap modulation in epitaxial halide perovskite nanowires Oksenberg, Eitan; Merdasa, Aboma; Houben, Lothar Nature Communications, Vol. 11, Issue 1 https://doi.org/10.1038/s41467-020-14365-2	journal	January 2020
PTFE-based microreactor system for the continuous synthesis of full-visible-spectrum emitting cesium lead halide perovskite nanocrystals Zhang, Chengxi; Luan, Weiling; Yin, Yuhang Beilstein Journal of Nanotechnology, Vol. 8 https://doi.org/10.3762/bjnano.8.252	journal	November 2017
Microcarrier-Assisted Inorganic Shelling of Lead Halide Perovskite Nanocrystals N., Dirin, Dmitry; M., Benin, Bogdan; Sergii, Yakunin, ETH Zurich https://doi.org/10.3929/ethz-b-000376105	text	January 2019

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