A rapid heating and high magnetic field thermal analysis technique

Kesler, Michael S.; McGuire, Michael A.; Conner, Ben; Rios, Orlando; Murphy, Bart; Carter, William; Henderson, Hunter B.; Ludtka, Gerard M.; Kisner, Roger A.

doi:10.1007/s10973-021-11010-y

Title: A rapid heating and high magnetic field thermal analysis technique

Journal Article · Sun Sep 05 00:00:00 EDT 2021 · Journal of Thermal Analysis and Calorimetry

DOI:https://doi.org/10.1007/s10973-021-11010-y· OSTI ID:1818785

; McGuire, Michael A.; Conner, Ben; Rios, Orlando; Murphy, Bart; Carter, William; Henderson, Hunter B.; Ludtka, Gerard M.; Kisner, Roger A.

Abstract A new thermal analysis technique is described that allows measurements to be performed on bulk samples at extreme heating and cooling rates and in high magnetic fields. High heating rates, up to 1000 °C min ⁻¹ , are achieved through electromagnetic induction heating of a custom-built apparatus fitted with commercial thermal analysis heads and sensor. Rapid cooling rates, up to 100 °C min ⁻¹ , are enabled by gas quenching and the small thermal mass of the induction furnace. The custom apparatus is designed to fit inside a superconducting magnet capable of fields up to 9 Tesla. This study demonstrates that the instrument is capable of collecting accurate thermal analysis data in high magnetic fields and rapidly acquiring data for dynamic processes. While the full potential of the technique is still unrealized, currently, it can provide insight into phenomena at time scales relevant to heat treatment in many industrial processes and into little understood effects of high magnetic field processing.

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Research Organization:: Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Energy Efficiency and Renewable Energy (EERE), Energy Efficiency Office. Advanced Manufacturing Office

Grant/Contract Number:: AC05-00OR22725; AC52-07NA27344

OSTI ID:: 1818785

Alternate ID(s):: OSTI ID: 1819615

Journal Information:: Journal of Thermal Analysis and Calorimetry, Journal Name: Journal of Thermal Analysis and Calorimetry Vol. 147 Journal Issue: 13; ISSN 1388-6150

Publisher:: Springer Science + Business MediaCopyright Statement

Country of Publication:: Hungary

Language:: English

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