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Quantitative texture analysis using the NOMAD time-of-flight neutron diffractometer

Journal Article · · Journal of Applied Crystallography (Online)

Strategies for efficient and reliable texture measurements have been explored using the Nanoscale Ordered Materials Diffractometer (NOMAD) at the Spallation Neutron Source located at Oak Ridge National Laboratory (ORNL). To test these strategies, the texture of an Al alloy was also investigated using another neutron diffraction instrument, a constant-wavelength neutron diffractometer (NRSF2) located at the High Flux Isotope Reactor, also at ORNL. Reasonable agreement was found across the two experimental methods, but differences in overall texture strength and the symmetry of some components were noted, depending on the data reduction and analysis method selected. Finally, on the basis of these results, potential improvements are identified which would enhance the texture measurement capability on NOMAD.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE; USDOE Office of Science (SC), Basic Energy Sciences (BES)
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
1810020
Journal Information:
Journal of Applied Crystallography (Online), Journal Name: Journal of Applied Crystallography (Online) Journal Issue: 3 Vol. 54; ISSN 1600-5767
Publisher:
International Union of CrystallographyCopyright Statement
Country of Publication:
United States
Language:
English

References (50)

A New Approach to More Realistic Rolling Texture Simulation journal April 2002
Berechnung der elastischen Konstanten des Vielkristalls aus den Konstanten des Einkristalls journal August 1958
Modeling texture change during the static recrystallization of interstitial free steels journal January 1996
Applications of TOF neutron diffraction in archaeometry journal March 2006
SMARTS - a spectrometer for strain measurement in engineering materials journal December 2002
A variational approach to the theory of the elastic behaviour of polycrystals journal October 1962
Choice of collimators for a crystal spectrometer for neutron diffraction journal October 1958
The SKAT texture diffractometer at the pulsed reactor IBR-2 at Dubna: experimental layout and first measurements
  • Ullemeyer, K.; Spalthoff, P.; Heinitz, J.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 412, Issue 1 https://doi.org/10.1016/S0168-9002(98)00340-4
journal June 1998
Texture inheritance and variant selection through an hcp–bcc–hcp phase transformation journal June 2010
Texture enhancement during grain growth of magnesium alloy AZ31B journal March 2015
Deformation texture prediction: from the Taylor model to the advanced Lamel model journal March 2005
Measuring and modeling the anisotropic, high strain rate deformation of Al alloy, 7085, plate in T711 temper journal June 2017
Texture analysis with the new HIPPO TOF diffractometer
  • Wenk, H. -R.; Lutterotti, L.; Vogel, S.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 515, Issue 3 https://doi.org/10.1016/j.nima.2003.05.001
journal December 2003
Mantid—Data analysis and visualization package for neutron scattering and μ SR experiments
  • Arnold, O.; Bilheux, J. C.; Borreguero, J. M.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 764 https://doi.org/10.1016/j.nima.2014.07.029
journal November 2014
The Nanoscale Ordered MAterials Diffractometer NOMAD at the Spallation Neutron Source SNS
  • Neuefeind, Jörg; Feygenson, Mikhail; Carruth, John
  • Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 287 https://doi.org/10.1016/j.nimb.2012.05.037
journal September 2012
Overview of the Conceptual Design of the Future VENUS Neutron Imaging Beam Line at the Spallation Neutron Source journal January 2015
Wombat: The high-intensity powder diffractometer at the OPAL reactor journal November 2006
Neutron texture analysis on GEM at ISIS journal November 2006
VULCAN—The engineering diffractometer at the SNS journal November 2006
Analytical description of rolling textures in face-centred-cubic metals journal March 2013
SciPy 1.0: fundamental algorithms for scientific computing in Python journal February 2020
Entropy optimization in quantitative texture analysis journal August 1988
Probing orientation information using 3-dimensional reciprocal space volume analysis journal January 2019
Current capabilities of the residual stress diffractometer at the high flux isotope reactor journal September 2018
The Elastic Behaviour of a Crystalline Aggregate journal May 1952
A quantitative evaluation of the deformation texture predictions for aluminium alloys from crystal plasticity finite element method journal July 2004
Quantitative Rietveld texture analysis of zirconium from single synchrotron diffraction images journal March 2005
Quantitative texture analysis with the HIPPO neutron TOF diffractometer journal May 2005
ENGIN-X: a third-generation neutron strain scanner journal November 2006
A novel pole figure inversion method: specification of the MTEX algorithm journal November 2008
Optimizing the experimental design of texture goniometry journal November 2012
GSAS-II : the genesis of a modern open-source all purpose crystallography software package journal March 2013
Profile shape functions in Rietveld refinements journal August 1982
Standard project for pole-figure determination by neutron diffraction journal October 1991
Practical aspects of calculating the elastic properties of polycrystals from the texture according to different models journal December 1992
Quantitative texture analysis by Rietveld refinement journal August 1997
A six-axis robotic sample changer for high-throughput neutron powder diffraction and texture measurements journal November 2014
Rapid measurement scheme for texture in cubic metallic materials using time-of-flight neutron diffraction at iMATERIA journal September 2016
High stereographic resolution texture and residual stress evaluation using time-of-flight neutron diffraction journal May 2018
Determination of pole figure coverage for texture measurements with neutron time-of-flight diffractometers journal June 2018
Rietveld texture analysis from TOF neutron diffraction data journal September 2010
Properties of Projection Lines in the Space of the Orientation Distribution Function journal January 1989
The ODF Approximation From Pole Figures With the Aid of the ADC Method journal January 1991
Minimal Pole Figure Ranges for Quantitative Texture Analysis journal January 1992
Deconvolution of Superposed Pole Figures by Discrete ODF Methods: Comparison of ADC and WIMV for Quartz and Calcite With Trigonal Crystal and Triclinic Specimen Symmetry journal January 1994
Evaluation of the Effect of Initial Texture on the Development of Deformation Texture journal January 1986
Metallurgical studies with the HIPPO diffractometer at LANSCE journal September 2014
Neutron Diffraction Texture Analysis journal January 2006
Texture Analysis from Diffraction Spectra journal May 1994
Texture Analysis with MTEX – Free and Open Source Software Toolbox journal February 2010

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