Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Nucleation and growth of tungsten nanotendrils grown under divertor-like conditions

Journal Article · · Journal of Nuclear Materials
Tungsten is the primary candidate for plasma-facing materials in the critical regions of a magnetic fusion energy (MFE) device, such as a tokamak. However, tungsten (and many other metals) grow copious nanotendril "fuzz" when exposed to fusion-relevant He-bearing plasmas, and the impact of this fuzz on reactor operation is still unknown. Further, the mechanism of fuzz growth is also poorly understood at present. In order to experimentally probe the growth mechanisms, we developed a new sample preparation technique to examine the interface of individual nanotendril roots with the substrate (substrate/tendril interface) using electron microscopy and measured the grain boundary character distributions (GBCDs) of substrate/tendril interfaces, the GBs within individual tendrils (tendril/tendril interfaces), and GBs within the substrate (substrate/substrate interfaces). We find the substrate/tendril and tendril/tendril GBCDs are essentially indistinguishable, but very different from the substrate/substrate GBCDs, which implies that tendril growth periodically forms new GBs at the substrate/tendril interface, and these GBs are pushed upward to become tendril/tendril interfaces within the fuzz mat. These results will help guide future computational modelling studies to elucidate the details of the growth mechanisms.
Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE Office of Science (SC); USDOE Office of Science (SC), Fusion Energy Sciences (FES)
Grant/Contract Number:
AC05-00OR22725; FG02-07ER54912
OSTI ID:
1777822
Alternate ID(s):
OSTI ID: 1548076
OSTI ID: 22752223
Journal Information:
Journal of Nuclear Materials, Journal Name: Journal of Nuclear Materials Journal Issue: 0 Vol. 509; ISSN 0022-3115
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English

References (35)

A classification of symmetrical grain boundaries journal August 1987
Deuterium retention in tungsten in dependence of the surface conditions journal March 2003
Mechanical properties of micro-sized copper bending beams machined by the focused ion beam technique journal September 2005
Characterizing deformed ultrafine-grained and nanocrystalline materials using transmission Kikuchi diffraction in a scanning electron microscope journal January 2014
Experimental identification for physical mechanism of fiber-form nanostructure growth on metal surfaces with helium plasma irradiation journal November 2015
Formation of helium induced nanostructure ‘fuzz’ on various tungsten grades journal September 2010
Sputtering properties of tungsten ‘fuzzy’ surfaces journal August 2011
Tungsten as material for plasma-facing components in fusion devices journal August 2011
TEM observation of the growth process of helium nanobubbles on tungsten: Nanostructure formation mechanism journal November 2011
Helium effects on tungsten under fusion-relevant plasma loading conditions journal July 2013
Comparison of tungsten nano-tendrils grown in Alcator C-Mod and linear plasma devices journal July 2013
Atomistic modeling of growth and coalescence of helium nano-bubbles in tungsten journal August 2015
Low energy and low fluence helium implantations in tungsten: Molecular dynamics simulations and experiments journal March 2016
Transmission Kikuchi diffraction in a scanning electron microscope: A review journal December 2016
Deuterium retention in tungsten after heavy ion damage and hydrogen isotope exchange in PISCES journal August 2014
Structural evolution of tungsten surface exposed to sequential low-energy helium ion irradiation and transient heat loading journal August 2017
Microstructure refinement of tungsten by surface deformation for irradiation damage resistance journal January 2014
Grain orientations and grain boundaries in tungsten nonotendril fuzz grown under divertor-like conditions journal January 2017
Orientation mapping of nanostructured materials using transmission Kikuchi diffraction in the scanning electron microscope journal September 2012
On the optimum resolution of transmission-electron backscattered diffraction (t-EBSD) journal January 2016
LAMDA: Irradiated-Materials Microscopy at Oak Ridge National Laboratory journal August 2015
Risks of “Cleaning” Electron Backscatter Diffraction Data journal March 2010
Morphologies of tungsten nanotendrils grown under helium exposure journal February 2017
Helium bubble bursting in tungsten journal December 2013
Molecular-dynamics analysis of mobile helium cluster reactions near surfaces of plasma-exposed tungsten journal October 2015
Geometry of asymmetrical grain boundaries journal July 1992
Formation process of tungsten nanostructure by the exposure to helium plasma under fusion relevant plasma conditions journal August 2009
Effect of He on D retention in W exposed to low-energy, high-fluence (D, He, Ar) mixture plasmas journal November 2011
Tungsten nano-tendril growth in the Alcator C-Mod divertor journal March 2012
Stick–slip behavior identified in helium cluster growth in the subsurface of tungsten: effects of cluster depth journal September 2015
Spatially dependent cluster dynamics modeling of microstructure evolution in low energy helium irradiated tungsten journal August 2014
Helium, hydrogen, and fuzz in plasma-facing materials journal October 2017
Transmission EBSD from 10 nm domains in a scanning electron microscope: TRANSMISSION EBSD IN THE SEM journal November 2011
Loop punching and bubble rupture causing surface roughening —A model for W fuzz growth journal January 2014
Effects of Steady-State Plasma Exposure on Tungsten Surface Cracking due to Elm-Like Pulsed Plasma Bombardment journal November 2011

Cited By (1)

He-ion induced surface morphology change and nanofuzz growth on hot tungsten surfaces journal December 2018

Similar Records

Grain orientations and grain boundaries in tungsten nonotendril fuzz grown under divertor-like conditions
Journal Article · Sun Sep 18 20:00:00 EDT 2016 · Scripta Materialia · OSTI ID:1326512

Morphologies of tungsten nanotendrils grown under helium exposure
Journal Article · Mon Feb 13 19:00:00 EST 2017 · Scientific Reports · OSTI ID:1344265

Helium diffusion and bubble evolution in tungsten nanotendrils
Journal Article · Mon Jul 13 20:00:00 EDT 2020 · Computational Materials Science · OSTI ID:1639053