Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

Liermann, H. P.; Konôpková, Z.; Appel, K.; Prescher, C.; Schropp, A.; Cerantola, V.; Husband, R. J.; McHardy, J. D.; McMahon, M. I.; McWilliams, R. S.; Pépin, C. M.; Mainberger, J.; Roeper, M.; Berghäuser, A.; Damker, H.; Talkovski, P.; Foese, M.; Kujala, N.; Ball, O. B.; Baron, M. A.; Briggs, R.; Bykov, M.; Bykova, E.; Chantel, J.; Coleman, A. L.; Cynn, H.; Dattelbaum, D.; Dresselhaus-Marais, L. E.; Eggert, J. H.; Ehm, L.; Evans, W. J.; Fiquet, G.; Frost, M.; Glazyrin, K.; Goncharov, A. F.; Hwang, H.; Jenei, Zs.; Kim, J. -Y.; Langenhorst, F.; Lee, Y.; Makita, M.; Marquardt, H.; McBride, E. E.; Merkel, S.; Morard, G.; O'Bannon, III, E. F.; Otzen, C.; Pace, E. J.; Pelka, A.; Pigott, J. S.; Prakapenka, V. B.; Redmer, R.; Sanchez-Valle, C.; Schoelmerich, M.; Speziale, S.; Spiekermann, G.; Sturtevant, B. T.; Toleikis, S.; Velisavljevic, N.; Wilke, M.; Yoo, C. -S.; Baehtz, C.; Zastrau, U.; Strohm, C.

doi:10.1107/S1600577521002551

Title: Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

Journal Article · Wed Apr 14 00:00:00 EDT 2021 · Journal of Synchrotron Radiation (Online)

DOI:https://doi.org/10.1107/S1600577521002551· OSTI ID:1777508

; Konôpková, Z.; Appel, K.; Prescher, C.; Schropp, A.; Cerantola, V.; Husband, R. J.; McHardy, J. D.; McMahon, M. I.; McWilliams, R. S.; Pépin, C. M.; Mainberger, J.; Roeper, M.; Berghäuser, A.; Damker, H.; Talkovski, P.; Foese, M.; Kujala, N.; Ball, O. B.; Baron, M. A. more »

The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump–probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.

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Research Organization:: SLAC National Accelerator Laboratory (SLAC), Menlo Park, CA (United States); Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: AC52-07 N A27344; 89233218CNA000001; 20190643DR; AC02-76SF00515; FWP100182; 864877; 670787; 730872; FOR 2440; NRF-2018R1A3B1052042; EP/P024513/1; EP/R02927X/1; NA0003342; DMR-1701360; W911NF-19–2-0172; W911NF-17–1-0468; EAR-1634415; AC52-07NA27344

OSTI ID:: 1777508

Alternate ID(s):: OSTI ID: 1788031; OSTI ID: 1867533

Report Number(s):: LLNL-JRNL-834744; JSYRES; PII: S1600577521002551

Journal Information:: Journal of Synchrotron Radiation (Online), Journal Name: Journal of Synchrotron Radiation (Online) Vol. 28 Journal Issue: 3; ISSN 1600-5775

Publisher:: International Union of Crystallography (IUCr)Copyright Statement

Country of Publication:: Denmark

Language:: English

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Title: Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

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