Synchrotron CT imaging of lattice structures with engineered defects

Patterson, Brian M.; Kuettner, Lindsey; Shear, Trevor; Henderson, Kevin; Herman, Matthew J.; Ionita, Axinte; Chawla, Nikhilesh; Williams, Jason; Sun, Tao; Fezzaa, Kamel; Xiao, Xianghui; Welch, Cynthia

doi:10.1007/s10853-020-04840-y

Synchrotron CT imaging of lattice structures with engineered defects

Journal Article · Wed May 27 00:00:00 EDT 2020 · Journal of Materials Science

DOI:https://doi.org/10.1007/s10853-020-04840-y· OSTI ID:1762695

^[1]; Kuettner, Lindsey ^[2]; Shear, Trevor ^[2]; Henderson, Kevin ^[2]; Herman, Matthew J. ^[2]; Ionita, Axinte ^[2]; Chawla, Nikhilesh ^[3]; Williams, Jason ^[3]; Sun, Tao ^[4]; Fezzaa, Kamel ^[4]; Xiao, Xianghui ^[4]; Welch, Cynthia ^[2]

Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Inst. for Materials Science, Los Alamos, NM (United States)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Arizona State Univ., Tempe, AZ (United States)
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Understanding mechanical failure, crack propagation, and compressive behavior at the micrometer scale is essential for tailoring material properties for structural performance in cellular materials. Typically, modeling of traditional polymer foam materials is clouded by the lack of control in material morphology and its inherent stochastic structure. Additive manufacturing with sub-micrometer resolution provides a direct path for experimenters to specifically tailor structures needed by modelers to explicitly probe mechanical performance. Using laboratory-based 3D X-ray computed tomographic imaging (CT), the examination of deformation and damage provides a critical path to understand how these soft materials behave. Additionally, synchrotron CT yields realistic information at higher strain rates to directly validate the robustness of our finite element modeling. For this study, nanolithographic printing was employed to generate a series of engineered lattices with increasing levels of defects through the random removal of ligaments. These structures were mechanically tested and imaged with laboratory-based microCT. Additionally, synchrotron experiments were conducted in which the structures were imaged in 3D at 14 Hz during compression at a 0.4 s^–1 strain rate. These 3D images show the changes in the structure as the ligaments bend, buckle and fracture in real time. This technique provides a robust framework for developing our methodologies and future exploration of engineered structures.

View Accepted Manuscript (DOE)

Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS); Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC)

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1762695

Journal Information:: Journal of Materials Science, Journal Name: Journal of Materials Science Journal Issue: 25 Vol. 55; ISSN 0022-2461

Publisher:: SpringerCopyright Statement

Country of Publication:: United States

Language:: English

References (35)

Design and Fabrication of Hollow Rigid Nanolattices via Two-Photon Lithography: Design and Fabrication of Hollow Rigid Nanolattices Montemayor, Lauren C.; Meza, Lucas R.; Greer, Julia R. Advanced Engineering Materials, Vol. 16, Issue 2 https://doi.org/10.1002/adem.201300254	journal	October 2013
Finite-element modeling of trabecular bone: Comparison with mechanical testing and determination of tissue modulus Ladd, Anthony J. C.; Kinney, John H.; Haupt, David L. Journal of Orthopaedic Research, Vol. 16, Issue 5 https://doi.org/10.1002/jor.1100160516	journal	September 1998
A review on 3D micro-additive manufacturing technologies Vaezi, Mohammad; Seitz, Hermann; Yang, Shoufeng The International Journal of Advanced Manufacturing Technology, Vol. 67, Issue 5-8 https://doi.org/10.1007/s00170-012-4605-2	journal	November 2012
20 Hz X-ray tomography during an in situ tensile test Maire, Eric; Le Bourlot, Christophe; Adrien, Jérôme International Journal of Fracture, Vol. 200, Issue 1-2 https://doi.org/10.1007/s10704-016-0077-y	journal	February 2016
Improving the fracture toughness of 3D printed thermoplastic polymers by fused deposition modeling Gardan, Julien; Makke, Ali; Recho, Naman International Journal of Fracture, Vol. 210, Issue 1-2 https://doi.org/10.1007/s10704-017-0257-4	journal	December 2017
The effects of strain rate, density, and temperature on the mechanical properties of polymethylene diisocyanate (PMDI)-based rigid polyurethane foams during compression Song, Bo; Lu, Wei-Yang; Syn, Chul Jin Journal of Materials Science, Vol. 44, Issue 2 https://doi.org/10.1007/s10853-008-3105-0	journal	January 2009
In situ X-ray synchrotron tomographic imaging during the compression of hyper-elastic polymeric materials Patterson, Brian M.; Cordes, Nikolaus L.; Henderson, Kevin Journal of Materials Science, Vol. 51, Issue 1 https://doi.org/10.1007/s10853-015-9355-8	journal	September 2015
Analysis of thermal history effects on mechanical anisotropy of 3D-printed polymer matrix composites via in situ X-ray tomography Mertens, J. C. E.; Henderson, K.; Cordes, N. L. Journal of Materials Science, Vol. 52, Issue 20 https://doi.org/10.1007/s10853-017-1339-4	journal	July 2017
The effect of grain size, strain rate, and temperature on the mechanical behavior of commercial purity aluminum Sun, P. L.; Cerreta, E. K.; Gray, G. T. Metallurgical and Materials Transactions A, Vol. 37, Issue 10 https://doi.org/10.1007/s11661-006-0180-1	journal	October 2006
A comparison among Neo-Hookean model, Mooney-Rivlin model, and Ogden model for chloroprene rubber Kim, Beomkeun; Lee, Seong Beom; Lee, Jayone International Journal of Precision Engineering and Manufacturing, Vol. 13, Issue 5 https://doi.org/10.1007/s12541-012-0099-y	journal	May 2012
Elastic constants of cellular structures Ladd, Anthony J. C.; Kinney, John H. Physica A: Statistical Mechanics and its Applications, Vol. 240, Issue 1-2 https://doi.org/10.1016/S0378-4371(97)00158-1	journal	June 1997
A novel theory of effective mechanical properties of closed-cell foam materials Ma, Yuli; Su, Xianyue; Pyrz, R. Acta Mechanica Solida Sinica, Vol. 26, Issue 6 https://doi.org/10.1016/S0894-9166(14)60001-X	journal	December 2013
Defect sensitivity of a 3D truss material Wallach, J. C.; Gibson, L. J. Scripta Materialia, Vol. 45, Issue 6 https://doi.org/10.1016/S1359-6462(01)01073-9	journal	September 2001
Finite element modelling of the actual structure of cellular materials determined by X-ray tomography Youssef, S.; Maire, E.; Gaertner, R. Acta Materialia, Vol. 53, Issue 3 https://doi.org/10.1016/j.actamat.2004.10.024	journal	February 2005
Mapping local deformation behavior in single cell metal lattice structures Carlton, Holly D.; Lind, Jonathan; Messner, Mark C. Acta Materialia, Vol. 129 https://doi.org/10.1016/j.actamat.2017.02.023	journal	May 2017
Hyperelastic strain measurements and constitutive parameters identification of 3D printed soft polymers by image processing Liljenhjerte, Johannes; Upadhyaya, Priyank; Kumar, S. Additive Manufacturing, Vol. 11 https://doi.org/10.1016/j.addma.2016.03.005	journal	July 2016
Influence of processing and orientation print effects on the mechanical and thermal behavior of 3D-Printed ULTEM® 9085 Material Zaldivar, R. J.; Witkin, D. B.; McLouth, T. Additive Manufacturing, Vol. 13 https://doi.org/10.1016/j.addma.2016.11.007	journal	January 2017
Additive manufacturing (3D printing): A review of materials, methods, applications and challenges Ngo, Tuan D.; Kashani, Alireza; Imbalzano, Gabriele Composites Part B: Engineering, Vol. 143 https://doi.org/10.1016/j.compositesb.2018.02.012	journal	June 2018
Cohesive finite element modeling of the delamination of HTPB binder and HMX crystals under tensile loading Walters, David J.; Luscher, Darby J.; Yeager, John D. International Journal of Mechanical Sciences, Vol. 140 https://doi.org/10.1016/j.ijmecsci.2018.02.048	journal	May 2018
Stress–strain behaviour of aluminium alloys at a wide range of strain rates Chen, Y.; Clausen, A. H.; Hopperstad, O. S. International Journal of Solids and Structures, Vol. 46, Issue 21 https://doi.org/10.1016/j.ijsolstr.2009.07.013	journal	October 2009
On the crushing response of random open-cell foams Gaitanaros, Stavros; Kyriakides, Stelios; Kraynik, Andrew M. International Journal of Solids and Structures, Vol. 49, Issue 19-20 https://doi.org/10.1016/j.ijsolstr.2012.03.003	journal	October 2012
Impact of material processing and deformation on cell morphology and mechanical behavior of polyurethane and nickel foams Burteau, A.; N’Guyen, F.; Bartout, J. D. International Journal of Solids and Structures, Vol. 49, Issue 19-20 https://doi.org/10.1016/j.ijsolstr.2012.05.026	journal	October 2012
Failure modes in high strength and stiffness to weight scaffolds produced by Selective Laser Melting Sercombe, Timothy B.; Xu, Xiaoxue; Challis, V. J. Materials & Design, Vol. 67 https://doi.org/10.1016/j.matdes.2014.10.063	journal	February 2015
The effect of varying strain rates and stress states on the plasticity, damage, and fracture of aluminum alloys Tucker, M. T.; Horstemeyer, M. F.; Whittington, W. R. Mechanics of Materials, Vol. 42, Issue 10 https://doi.org/10.1016/j.mechmat.2010.07.003	journal	October 2010
Effect of temperature and strain rate on the tensile deformation of polyamide 6 Shan, Gui-Fang; Yang, Wei; Yang, Ming-bo Polymer, Vol. 48, Issue 10 https://doi.org/10.1016/j.polymer.2007.03.013	journal	May 2007
Mapping internal deformation fields in 3D printed porous structure with digital volume correlation Wang, Bo; Sun, Lijuan; Pan, Bing Polymer Testing, Vol. 78 https://doi.org/10.1016/j.polymertesting.2019.105945	journal	September 2019
Cellular Solids Gibson, Lorna J.; Ashby, Michael F. Cambridge University Press https://doi.org/10.1017/CBO9781139878326	book	January 2014
Reactive, anomalous compression in shocked polyurethane foams Dattelbaum, Dana M.; Coe, Joshua D.; Kiyanda, Charles B. Journal of Applied Physics, Vol. 115, Issue 17 https://doi.org/10.1063/1.4875478	journal	May 2014
TomoPy: a framework for the analysis of synchrotron tomographic data Gürsoy, Dogˇa; De Carlo, Francesco; Xiao, Xianghui Journal of Synchrotron Radiation, Vol. 21, Issue 5 https://doi.org/10.1107/S1600577514013939	journal	August 2014
Fast iterative reconstruction of data in full interior tomography Arcadu, F.; Marone, F.; Stampanoni, M. Journal of Synchrotron Radiation, Vol. 24, Issue 1 https://doi.org/10.1107/S1600577516015794	journal	January 2017
Ultralight, ultrastiff mechanical metamaterials Zheng, X.; Lee, H.; Weisgraber, T. H. Science, Vol. 344, Issue 6190 https://doi.org/10.1126/science.1252291	journal	June 2014
Continuous liquid interface production of 3D objects Tumbleston, J. R.; Shirvanyants, D.; Ermoshkin, N. Science, Vol. 347, Issue 6228 https://doi.org/10.1126/science.aaa2397	journal	March 2015
Rapid, large-volume, thermally controlled 3D printing using a mobile liquid interface Walker, David A.; Hedrick, James L.; Mirkin, Chad A. Science, Vol. 366, Issue 6463 https://doi.org/10.1126/science.aax1562	journal	October 2019
Quantitative X-ray tomography Maire, E.; Withers, P. J. International Materials Reviews, Vol. 59, Issue 1 https://doi.org/10.1179/1743280413Y.0000000023	journal	December 2013
In Situ Imaging during Compression of Plastic Bonded Explosives for Damage Modeling Manner, Virginia W.; Yeager, John D.; Patterson, Brian M. Materials, Vol. 10, Issue 6 https://doi.org/10.3390/ma10060638	journal	June 2017

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