Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Improved Capacity Retention of Lithium Ion Batteries under Fast Charge via Metal-Coated Graphite Electrodes

Journal Article · · Journal of the Electrochemical Society (Online)

A primary barrier preventing repetitive fast charging of Li-ion batteries is lithium metal plating at the graphite anode. One approach toward mitigating Li metal deposition is the deliberate modification of the graphite anode surface with materials demonstrating high overpotentials unfavorable for Li metal nucleation, such as Ni or Cu nanoscale films. This research explores Ni and Cu surface coatings at different areal loadings (3 or 11 μg cm-2) on the electrochemistry of graphite/LiNi0.6Mn0.2Co0.2O2 (NMC622) type Li-ion batteries. Extended galvanostatic cycling of control and metal-coated electrodes in graphite/NMC622 pouch cells are conducted under high rate conditions. Based on the overpotential of Li deposition on metal foil, both Ni and Cu treatments were anticipated to result in reduced lithium deposition. The higher metal film loadings of 11 μg cm-2 Ni- or Cu-coated electrodes exhibit the highest capacity retention after 500 cycles, with mean improvements of 8% and 9%, respectively, over uncoated graphite electrodes. Li plating quantified by X-ray diffraction indicates that the metal films effectively reduce the quantity of plated Li compared to untreated electrodes, with 11 μg cm-2 Cu providing the greatest benefit.

Research Organization:
Brookhaven National Laboratory (BNL), Upton, NY (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
Grant/Contract Number:
SC0012704
OSTI ID:
1756178
Report Number(s):
BNL--220765-2020-JAAM
Journal Information:
Journal of the Electrochemical Society (Online), Journal Name: Journal of the Electrochemical Society (Online) Journal Issue: 16 Vol. 167; ISSN 1945-7111
Publisher:
IOP PublishingCopyright Statement
Country of Publication:
United States
Language:
English

References (65)

Enabling Rapid Charging Lithium Metal Batteries via Surface Acoustic Wave‐Driven Electrolyte Flow journal April 2020
Application of Alternating Current Scanning Electrochemical Microscopy in Lithium‐Ion Batteries: Local Visualization of the Electrode Surface journal September 2019
Investigation of Copper Corrosion Inhibition with Frequency-Dependent Alternating-Current Scanning Electrochemical Microscopy journal May 2012
Interfacial Properties of Copper-coated Graphite Electrodes: Coating Thickness Dependence journal June 2009
Thermal Conductivity of Small Nickel Particles journal February 2006
Development and application of a multipurpose electrodeposition cell configuration for studying plating processes on wafer specimen and for characterizing surface films by scanning electrochemical microscopy journal October 2017
Material contrast studies of conductive thin films on semiconductor substrates using scanning electrochemical microscopy journal February 2019
Improving Li-ion battery charge rate acceptance through highly ordered hierarchical electrode design journal March 2018
Thickness dependent electrical resistivity of ultrathin (<40 nm) Cu films journal March 2001
Experimental investigation of the lithium-ion battery impedance characteristic at various conditions and aging states and its influence on the application journal February 2013
High resolution constant-distance mode alternating current scanning electrochemical microscopy (AC-SECM) journal March 2004
Alternating current (AC) impedance imaging with combined atomic force scanning electrochemical microscopy (AFM-SECM) journal June 2007
Hydrogen mapping in an aluminum alloy using an alternating current scanning electrochemical microscope (AC-SECM) journal July 2017
Scanning electrochemical microscopy to study the effect of crystallographic orientation on the electrochemical activity of pure copper journal January 2014
Influence of local lithium metal deposition in 3D microstructures on local and global behavior of Lithium-ion batteries journal May 2016
Lithium-ion battery fast charging: A review journal August 2019
Asymmetric Temperature Modulation for Extreme Fast Charging of Lithium-Ion Batteries journal December 2019
From silver nanoparticles to thin films: Evolution of microstructure and electrical conduction on glass substrates journal February 2009
Electrochemical investigation of polarization phenomena and intercalation kinetics of oxidized graphite electrodes coated with evaporated metal layers journal June 2008
Increased cycling efficiency and rate capability of copper-coated silicon anodes in lithium-ion batteries journal January 2011
Equivalent circuit model parameters of a high-power Li-ion battery: Thermal and state of charge effects journal May 2011
Physical characterization of the charging process of a Li-ion battery and prediction of Li plating by electrochemical modelling journal January 2014
Quantification of bottlenecks to fast charging of lithium-ion-insertion cells for electric vehicles journal December 2014
Enabling fast charging – A battery technology gap assessment journal November 2017
Li plating as unwanted side reaction in commercial Li-ion cells – A review journal April 2018
Modeling and simulation of resistivity of nanometer scale copper journal July 2006
The crossover between tunnel and hopping conductivity in granulated films of noble metals journal November 2017
Quantum size effect in conductive properties of silver nanofilms journal September 2020
The Powder Diffraction File: a quality materials characterization database journal November 2019
Scanning electrochemical microscopy. Introduction and principles journal January 1989
Localized Electrochemical Impedance Spectroscopy: Visualization of Spatial Distributions of the Key Parameters Describing Solid/Liquid Interfaces journal January 2013
Inhomogeneous Degradation of Graphite Anodes in Li-Ion Cells: A Postmortem Study Using Glow Discharge Optical Emission Spectroscopy (GD-OES) journal September 2016
Mapping Electrochemical Heterogeneity at Iron Oxide Surfaces: A Local Electrochemical Impedance Study journal December 2015
Nanoscale Nucleation and Growth of Electrodeposited Lithium Metal journal January 2017
Anode Overpotential Control via Interfacial Modification: Inhibition of Lithium Plating on Graphite Anodes journal November 2019
Quantum Confinement and Its Related Effects on the Critical Size of GeO 2 Nanoparticles Anodes for Lithium Batteries journal January 2014
Selective deposition and stable encapsulation of lithium through heterogeneous seeded growth journal February 2016
Design principles for electrolytes and interfaces for stable lithium-metal batteries journal September 2016
In situ NMR observation of the formation of metallic lithium microstructures in lithium batteries journal May 2010
Challenges and opportunities towards fast-charging battery materials journal June 2019
Understanding undesirable anode lithium plating issues in lithium-ion batteries journal January 2016
Lithiation of multilayer Ni/NiO electrodes: criticality of nickel layer thicknesses on conversion reaction kinetics journal January 2017
Revealing the electronic character of the positive electrode/electrolyte interface in lithium-ion batteries journal January 2017
Alternating current techniques in scanning electrochemical microscopy (AC-SECM) journal January 2008
Exploring the interfaces between metal electrodes and aqueous electrolytes with electrochemical impedance spectroscopy journal January 2013
Kinetics of rapid electrode reactions journal January 1947
Electrical transport in metallic films journal March 2004
Electron mean free path in elemental metals journal February 2016
Scanning electrochemical microscope characterization of thin film combinatorial libraries for fuel cell electrode applications journal December 2004
Quantum size and surface effects in the electrical resistivity and high-energy electron reflectivity of ultrathin lead films journal September 1988
Theory of quantum size effects in thin Pb(111) films journal December 2002
Quantum size effects in metal nanofilms: Comparison of an electron-gas model and density functional theory calculations journal October 2009
Alteration of Cu conductivity in the size effect regime
  • Rossnagel, S. M.; Kuan, T. S.
  • Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures, Vol. 22, Issue 1 https://doi.org/10.1116/1.1642639
journal January 2004
Nanostructure and conductivity of thin metal films journal March 2004
Li Mass Transfer Through a Metallic Copper Film on a Carbon Fiber during the Electrochemical Insertion/Extraction Reaction journal January 2001
Mathematical Modeling of the Lithium Deposition Overcharge Reaction in Lithium-Ion Batteries Using Carbon-Based Negative Electrodes journal January 1999
Ni-Composite Microencapsulated Graphite as the Negative Electrode in Lithium-Ion Batteries II: Electrochemical Impedance and Self-Discharge Studies journal January 2000
Thin Ag Layer Inserted GZO Multilayer Grown by Roll-to-Roll Sputtering for Flexible and Transparent Conducting Electrodes journal January 2010
A Critical Review of Thermal Issues in Lithium-Ion Batteries journal January 2011
(Invited) Investigation of Early Degradation Processes at Coated Metals by AC-Scanning Electrochemical Microscopy journal May 2012
Detection of Li Deposition by Glow Discharge Optical Emission Spectroscopy in Post-Mortem Analysis journal January 2015
Optimizing Areal Capacities through Understanding the Limitations of Lithium-Ion Electrodes journal November 2015
Effects of Electrolyte Additives and Solvents on Unwanted Lithium Plating in Lithium-Ion Cells journal January 2017
Scanning Electrochemical Microscopy book January 2012
Impact of the Regularization Parameter in the Mean Free Path Reconstruction Method: Nanoscale Heat Transport and Beyond journal March 2019

Similar Records

Operando Synchrotron Studies of Inhomogeneity during Anode-Free Plating of Li Metal in Pouch Cell Batteries
Journal Article · Sun Feb 27 23:00:00 EST 2022 · Journal of the Electrochemical Society · OSTI ID:1860226

Related Subjects