Possibility of an integrated transmission electron microscope: enabling complex in-situ experiments

Hattar, Khalid; Jungjohann, Katherine L.

doi:10.1007/s10853-020-05598-z

Title: Possibility of an integrated transmission electron microscope: enabling complex in-situ experiments

Journal Article · Sun Jan 03 00:00:00 EST 2021 · Journal of Materials Science

DOI:https://doi.org/10.1007/s10853-020-05598-z· OSTI ID:1755444

; Jungjohann, Katherine L.

Abstract Multimodal in-situ experiments are the wave of the future, as this approach will permit multispectral data collection and analysis during real-time nanoscale observation. In contrast, the evolution of technique development in the electron microscopy field has generally trended toward specialization and subsequent bifurcation into more and more niche instruments, creating a challenge for reintegration and backward compatibility for in-situ experiments on state-of-the-art microscopes. We do not believe this to be a requirement in the field; therefore, we propose an adaptive instrument that is designed to allow nearly simultaneous collection of data from aberration-corrected transmission electron microscopy (TEM), probe-corrected scanning transmission electron microscopy, ultrafast TEM, and dynamic TEM with a flexible in-situ testing chamber, where the entire instrument can be modified as future technologies are developed. The value would be to obtain a holistic understanding of the underlying physics and chemistry of the process-structure–property relationships in materials exposed to controlled extreme environments. Such a tool would permit the ability to explore, in-situ, the active reaction mechanisms in a controlled manner emulating those of real-world applications with nanometer and nanosecond resolution. If such a powerful tool is developed, it has the potential to revolutionize our materials understanding of nanoscale mechanisms and transients. Graphical Abstract

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Research Organization:: Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: FWP-14-013311; AC04-94AL85000; NA0003525

OSTI ID:: 1755444

Alternate ID(s):: OSTI ID: 1765774

Report Number(s):: SAND-2021-0687J; PII: 5598

Journal Information:: Journal of Materials Science, Journal Name: Journal of Materials Science Vol. 56 Journal Issue: 9; ISSN 0022-2461

Publisher:: SpringerCopyright Statement

Country of Publication:: United States

Language:: English

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