Conducting reactions in Leidenfrost-levitated droplets

Cooks, Robert Graham; Pulliam, Christopher; Bain, Ryan M.

Title: Conducting reactions in Leidenfrost-levitated droplets

Patent · Tue Sep 15 00:00:00 EDT 2020

OSTI ID:1735255

Cooks, Robert Graham; Pulliam, Christopher; Bain, Ryan M.

The invention generally relates to conducting reactions in Leidenfrost-levitated droplets.

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Research Organization:: Purdue Univ., West Lafayette, IN (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: FG02-06ER15807

Assignee:: Purdue Research Foundation (West Lafayette, IN)

Patent Number(s):: 10,774,044

Application Number:: 15/613,520

OSTI ID:: 1735255

Resource Relation:: Patent File Date: 06/05/2017

Country of Publication:: United States

Language:: English

References (16)

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Dynamics of Field-Induced Droplet Ionization: Time-Resolved Studies of Distortion, Jetting, and Progeny Formation from Charged and Neutral Methanol Droplets Exposed to Strong Electric Fields Grimm, Ronald L.; Beauchamp, J. L. The Journal of Physical Chemistry B, Vol. 109, Issue 16 https://doi.org/10.1021/jp0450540	journal	April 2005
Some Investigations on the Deformation and Breaking of Water Drops in Strong Electric Fields Macky, W. A. Proceedings of the Royal Society A: Mathematical, Physical and Engineering Sciences, Vol. 133, Issue 822 https://doi.org/10.1098/rspa.1931.0168	journal	October 1931
The bursting of soap-bubbles in a uniform electric field Wilson, C. T. R.; Taylor, G. I. Mathematical Proceedings of the Cambridge Philosophical Society, Vol. 22, Issue 5 https://doi.org/10.1017/S0305004100009609	journal	July 1925
Accelerated CarbonCarbon Bond-Forming Reactions in Preparative Electrospray Müller, Thomas; Badu-Tawiah, Abraham; Cooks, R. Graham Angewandte Chemie International Edition, Vol. 51, Issue 47 https://doi.org/10.1002/anie.201206632	journal	October 2012
Green chemistry and nanofabrication in a levitated Leidenfrost drop Abdelaziz, Ramzy; Disci-Zayed, Duygu; Hedayati, Mehdi Keshavarz Nature Communications, Vol. 4, Issue 1 https://doi.org/10.1038/ncomms3400	journal	October 2013
Mass Spectrometry in Organic Synthesis: Claisen–Schmidt Base-Catalyzed Condensation and Hammett Correlation of Substituent Effects Bain, Ryan M.; Pulliam, Christopher J.; Yan, Xin Journal of Chemical Education, Vol. 91, Issue 11 https://doi.org/10.1021/ed500288m	journal	July 2014
Syntheses of Isoquinoline and Substituted Quinolines in Charged Microdroplets Banerjee, Shibdas; Zare, Richard N. Angewandte Chemie International Edition, Vol. 54, Issue 49 https://doi.org/10.1002/anie.201507805	journal	October 2015
Probing Interfacial Chemistry of Single Droplets with Field-Induced Droplet Ionization Mass Spectrometry: Physical Adsorption of Polycyclic Aromatic Hydrocarbons and Ozonolysis of Oleic Acid and Related Compounds Grimm, Ronald L.; Hodyss, Robert; Beauchamp, J. L. Analytical Chemistry, Vol. 78, Issue 11, p. 3800-3806 https://doi.org/10.1021/ac0601922	journal	June 2006
Practical implications of some recent studies in electrospray ionization fundamentals Cech, Nadja B.; Enke, Christie G. Mass Spectrometry Reviews, Vol. 20, Issue 6, p. 362-387 https://doi.org/10.1002/mas.10008	journal	January 2001
Accelerated bimolecular reactions in microdroplets studied by desorption electrospray ionization mass spectrometry Girod, Marion; Moyano, Encarnacion; Campbell, Dahlia I. Chem. Sci., Vol. 2, Issue 3 https://doi.org/10.1039/C0SC00416B	journal	January 2011
Chemical Reactivity Assessment Using Reactive Paper Spray Ionization Mass Spectrometry: The Katritzky Reaction Yan, Xin; Augusti, Rodinei; Li, Xin ChemPlusChem, Vol. 78, Issue 9 https://doi.org/10.1002/cplu.201300172	journal	August 2013
Reducing-Agent-Free Instant Synthesis of Carbon-Supported Pd Catalysts in a Green Leidenfrost Droplet Reactor and Catalytic Activity in Formic Acid Dehydrogenation Lee, Dong-Wook; Jin, Min-Ho; Lee, Young-Joo Scientific Reports, Vol. 6, Issue 1 https://doi.org/10.1038/srep26474	journal	May 2016
Accelerated Hantzsch electrospray synthesis with temporal control of reaction intermediates Bain, Ryan M.; Pulliam, Christopher J.; Cooks, R. Graham Chemical Science, Vol. 6, Issue 1 https://doi.org/10.1039/C4SC02436B	journal	January 2015
Unraveling the Mechanism of Electrospray Ionization Konermann, Lars; Ahadi, Elias; Rodriguez, Antony D. Analytical Chemistry, Vol. 85, Issue 1 https://doi.org/10.1021/ac302789c	journal	November 2012
Straightforward Synthesis of Metal Nanoparticles and Hierarchical Porous Metals Assisted by Partial Film Boiling Phenomena Lee, Dong-Wook; Jin, Min-Ho; Lee, Chun-Boo Chemistry of Materials, Vol. 27, Issue 15 https://doi.org/10.1021/acs.chemmater.5b00143	journal	July 2015

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