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Title: Transient Microstructure Evolutions and Local Properties of Dual-Phase 980 MPa Grade Steel Via Friction Stir Spot Processing

Journal Article · · Materials
DOI:https://doi.org/10.3390/ma13194406· OSTI ID:1669766

Friction stir processing is a novel solid-state process to modify microstructures and their properties by intense, localized plastic deformation. However, little research has been reported for microstructure evolutions of advanced high-strength steels during the process. The present work focuses on the study of transient microstructure changes and local mechanical properties for friction stir spot processed dual-phase (DP) 980 MPa grade steel (DP980) under different peak temperatures. A pinless silicon nitride ceramic tool was used to produce relatively simple material deformation and flow near the tool. Friction stir spot processed steel samples were characterized by optical and electron microscopies. Furthermore, Vickers microhardness and nano-indentation measurements were used to study local mechanical properties for correlation with microstructures. A swallow layer of refined grains (<0.6 µm) was obtained with a low peak temperature (under 400 °C), whereas higher peak temperatures (>Ac1) led to a change in grain size with different microstructures (fine-grained DP or martensite). Electron back-scattered diffraction characterizations revealed a large deformation in the as-received microstructures (mixture of ferrite and tempered martensite) induced by friction stir spot processing, leading to recrystallization and grain refinement around the stirred zone. Also, nano-indentation measurements showed a higher hardness than the hardness of the as-received DP980. Friction stir processing with different process conditions effectively changed microstructures and local mechanical properties.

Research Organization:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE Office of Energy Efficiency and Renewable Energy (EERE); JFE Steel Corporation
Grant/Contract Number:
AC05-00OR22725; NFE-17-06928
OSTI ID:
1669766
Journal Information:
Materials, Vol. 13, Issue 19; ISSN 1996-1944
Publisher:
MDPICopyright Statement
Country of Publication:
United States
Language:
English

References (29)

Numerical modelling and experimental investigation of thermal and material flow in probeless friction stir spot welding process of Al 2198-T8 journal May 2018
Dynamic and post-dynamic recrystallization under hot, cold and severe plastic deformation conditions journal March 2014
Microstructural characterisation of double pulse resistance spot welded advanced high strength steel journal January 2017
Temperature-dependent emissivity of silicon-related materials and structures journal January 1998
A Dislocation-Based Theory for the Deformation Hardening Behavior of DP Steels: Impact of Martensite Content and Ferrite Grain Size journal January 2010
Friction stir spot welding of DP780 carbon steel journal May 2010
Experimental and numerical study on geometrically necessary dislocations and non-homogeneous mechanical properties of the ferrite phase in dual phase steels journal June 2011
Grain size and particle dispersion effects on the tensile behavior of friction stir welded MA956 oxide dispersion strengthened steel from low to elevated temperatures journal January 2014
Projection friction stir spot welding: a pathway to produce strong keyhole-free welds journal September 2018
Strengthening Mechanisms of Ultrafine Grained Dual Phase Steels Developed by New Thermomechanical Processing journal January 2015
Modelling and visualisation of material flow in friction stir spot welding journal November 2015
A study on heat affected zone softening in resistance spot welded dual phase steel by nanoindentation journal December 2009
Development of Friction Stir Welding (FSW) of High Strength Steel Sheet [高張力薄鋼板の摩擦攪拌接合(FSW)技術の開発] journal January 2009
Correlation of Yield Strength and Tensile Strength with Hardness for Steels journal April 2008
Overview Inclusion assisted microstructure control in C–Mn and low alloy steel welds journal August 2005
Effect of friction stir processing on microstructure and work hardening behavior of reduced activation ferritic/martensitic steel journal January 2019
Nanoindentation study of ferrite–martensite dual phase steels developed by a new thermomechanical processing journal July 2015
Friction stir processing of dual phase steel: Microstructural evolution and mechanical properties journal September 2019
Calculation of Critical Temperatures by Empirical Formulae journal June 2016
HAZ Microstructures and Local Mechanical Properties of High Strength Steels Resistance Spot Welds journal January 2011
Effects of process parameters on friction self-piercing riveting of dissimilar materials journal November 2016
Microstructure and morphology evolution of probeless friction stir spot welded joints of aluminum alloy journal February 2018
Separation of size-dependent strengthening contributions in fine-grained Dual Phase steels by nanoindentation journal July 2006
Microstructure and mechanical properties of hard zone in friction stir welded X80 pipeline steel relative to different heat input journal December 2013
Microstructure and properties in friction stir weld of 12Cr steel journal December 2013
Friction stir based welding and processing technologies - processes, parameters, microstructures and applications: A review journal January 2018
Nanoindentation and microstructure analysis of resistance spot welded dual phase steel journal January 2010
Friction stir welding of AISI 1080 steel using liquid CO 2 for enhanced toughness and ductility journal August 2013
Feasibility of friction stir welding steel journal December 1999

Figures / Tables (21)


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