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Title: Binder jet 3D printing—Process parameters, materials, properties, modeling, and challenges

Journal Article · · Progress in Materials Science

As a non-beam-based additive manufacturing (AM) method, binder jet 3D printing (BJ3DP) is a process where a liquid binder is jetted on layers of powdered materials, selectively joined and then followed by densification process. Among AM technologies, binder jetting holds distinctive promise due to possibility of rapid production of complex structures to achieve isotropic properties in the 3D printed samples. By taking advantage of traditional powder metallurgy, BJ3DP machines can produce prototypes in which material properties and surface finish are similar to those attained with traditional powder metallurgy. Various powdered materials have been 3D printed, however, a typical challenge during BJ3DP is developing printing and post-processing methods that maximize part performance. Therefore, a detailed review of the physical processes during 3D printing and the fundamental science of densification after sintering and post heat treatment steps are provided to understand the microstructural evolution and properties of binder jetted parts. Further, to determine the effects of the binder jetting process on metallurgical properties, the role of powder characteristics (e.g. morphology, mean size, and distribution), printing process parameters (e.g. layer thickness, print orientation, binder saturation, print speed, and drying time), sintering (e.g. temperature and holding time) and post-processing are discussed. With the development of AM technologies and need for post-processing in 3D printed parts, it is necessary to understand the microstructural evolution during densification process and here, processing steps are explained. Finally, opportunities for future advancement are addressed.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE Office of Energy Efficiency and Renewable Energy (EERE)
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
1763858
Alternate ID(s):
OSTI ID: 1649188
Journal Information:
Progress in Materials Science, Journal Name: Progress in Materials Science Vol. 119 Journal Issue: C; ISSN 0079-6425
Publisher:
ElsevierCopyright Statement
Country of Publication:
United Kingdom
Language:
English

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Effect of particle size on three dimensional printed mesh structures journal June 2009
Quantification of powder wetting by drop penetration time journal April 2015
3D printing of hydroxyapatite: Effect of binder concentration in pre-coated particle on part strength journal May 2007
Interfacial characteristic and mechanical performance of maraging steel-copper functional bimetal produced by selective laser melting based hybrid manufacture journal October 2018
Additive manufacturing and postprocessing of Ti-6Al-4V for superior mechanical properties journal October 2016
Contact angle, wetting, and adhesion: a critical review journal January 1992
Additive manufacturing of WC-20Co components by 3D gel-printing journal January 2018
Joining of Inconel 718 and 316 Stainless Steel using electron beam melting additive manufacturing technology journal March 2016
Fabrication of barium titanate by binder jetting additive manufacturing technology journal June 2015
Effects of layer thickness and binder saturation level parameters on 3D printing process journal July 2010
Determination of structural and magnetic properties in directionally solidified Ni-Mn-Ga rod with an axial compositional variation journal November 2017
Three-dimensional printing of hard materials journal February 2020
3D printing of porcelain by layerwise slurry deposition journal August 2018
Microstructural Evaluation of Magnetocaloric Ni-Co-Mn-Sn Produced by Directed Energy Deposition journal July 2016
Molecular dynamics simulation and experimental study of the bonding properties of polymer binders in 3D powder printed hydroxyapatite bioceramic bone scaffolds journal November 2017
Binder jetting additive manufacturing of aluminum nitride components journal August 2019
3D printing of bone substitute implants using calcium phosphate and bioactive glasses journal September 2010
Effects of Heat Treatment on the Mechanical and Degradation Properties of 3D-Printed Calcium-Sulphate-Based Scaffolds journal January 2013
Modeling the granule formation mechanism from single drop impact on a powder bed journal March 2013
Effect of moisture and magnesium stearate concentration on flow properties of cohesive granular materials journal May 2007
Design guidelines for laser additive manufacturing of lightweight structures in TiAl6V4 journal February 2015
The fabrication of metal matrix composites by a pressureless infiltration technique journal January 1991
Characterization of particulate matters and total VOC emissions from a binder jetting 3D printer journal November 2015
Osteoconduction and osteoinduction of low-temperature 3D printed bioceramic implants journal March 2008
Binder Jet 3D Printing of 316L Stainless Steel: Effects of HIP on Fatigue journal August 2019
Single asperity nanoscratch behaviour of HIPed and cast Stellite 6 alloys journal April 2014
On the adhesive JKR contact and rolling models for reduced particle stiffness discrete element simulations journal September 2017
A comparison of tensile failure in 3D-printed and natural sandstone journal August 2017
Sintering processes of two nanoparticles: A study by molecular dynamics simulations journal January 1996
Three-Dimensional Printing of Ti3SiC2-Based Ceramics: Rapid Communications of the American Ceramic Society journal February 2011
Bone response to 3D periodic hydroxyapatite scaffolds with and without tailored microporosity to deliver bone morphogenetic protein 2 journal January 2005
A Phase Field Model of Sintering with Direction-Dependent Diffusion journal January 2012
The mechanism of densification during sintering of metallic particles journal January 1956
Functionally graded Inconel 718 processed by additive manufacturing: Crystallographic texture, anisotropy of microstructure and mechanical properties journal January 2017
On the Spreading of Liquids on Solid Surfaces: Static and Dynamic Contact Lines journal January 1979
Effect of Particle Size Distribution on Powder Packing and Sintering in Binder Jetting Additive Manufacturing of Metals journal June 2017
Implementation of a phase field model for simulating evolution of two powder particles representing microstructural changes during sintering journal December 2017
Steel Parts with Tailored Material Gradients by 3D-Printing Using Nano-Particulate Ink journal August 2005
Wettability of tungsten carbide by liquid binders in WC–Co cemented carbides: Is it complete for all carbon contents? journal January 2017
Additive manufacturing of metallic components – Process, structure and properties journal March 2018
Dynamic wetting angle of a spreading droplet journal August 2005
Effect of Mn incorporation for Ni on the properties of melt spun off-stoichiometric compositions of NiMnGa alloys journal May 2011
An improved integral non-linear model for the contact of particles in distinct element simulations journal March 2005
Industrial Additive Manufacturing: A manufacturing systems perspective journal November 2017
Binder-jet powder-bed additive manufacturing (3D printing) of thick graphene-based electrodes journal August 2017
Description of agglomerate growth journal July 1998
A novel method to fabricate TiAl intermetallic alloy 3D parts using additive manufacturing journal April 2017
Synthesis of the In Situ Nb-Si Composites by Binder Jetting Additive Manufacturing Technology journal September 2019
Entrapment of air during imbibition of agglomerated powder beds journal May 2017
Effect of Gray Scale Binder Levels on Additive Manufacturing of Porous Scaffolds with Heterogeneous Properties journal September 2014
Energy and Material Flow Analysis of Binder-jetting Additive Manufacturing Processes journal January 2014
Piezo-Plunger Jetting Technology: An Experimental Study on Jetting Characteristics of Filled Epoxy Polymers journal February 2019
Models, algorithms and validation for opensource DEM and CFD-DEM journal January 2012
Additive manufacturing of metallic cellular materials via three-dimensional printing journal July 2010
Interstitial elements in titanium powder metallurgy: sources and control journal July 2011
Effect of enhanced interfacial reaction on the microstructure, phase transformation and mechanical property of Ni–Mn–Ga particles/Mg composites journal October 2015
High resolution pore size analysis in metallic powders by X-ray tomography journal November 2016
3D-printed rib-enforced shell sand mold for aluminum castings journal February 2018
The Effect of Moisture on Powder Flow and on Compaction and Physical Stability of Tablets journal January 1989
Life Cycle Assessment of 3D Printed Products in a Distributed Manufacturing System: LCA-Distributed Manufacturing System journal June 2017
Effect of the oxygen content in solution on the static and cyclic deformation of titanium foams journal June 2009
Dissolutive Capillary Penetration with Expanding Pores and Transient Contact Angles journal November 2000
Wear properties of sintered WC-12%Co processed via Binder Jet 3D Printing (BJ3DP) journal January 2019
Influence of grain size and grain-size distribution on workability of granules with 3D printing journal August 2013
The role of shell/core saturation level on the accuracy and mechanical characteristics of porous calcium phosphate models produced by 3Dprinting journal January 2015
Dynamic contact angle modeling of droplet reattachment at the gas channel wall in polymer electrolyte fuel cells journal August 2019
Drop Penetration into Porous Powder Beds journal September 2002
Influence of printing parameters on the transformation efficiency of 3D‐printed plaster of paris to hydroxyapatite and its properties journal September 2012
An experimental study into the effects of bulk and flow behaviour of laser sintering polymer powders on resulting part properties journal January 2015
Additive Manufacturing Processes: Selective Laser Melting, Electron Beam Melting and Binder Jetting—Selection Guidelines journal June 2017
3D print of polymer bonded rare-earth magnets, and 3D magnetic field scanning with an end-user 3D printer journal October 2016
Ceramic binder jetting additive manufacturing: Particle coating for increasing powder sinterability and part strength journal January 2019
The influence of powder apparent density on the density in direct laser-sintered metallic parts journal February 2007
Microstructural evolution and mechanical properties of differently heat-treated binder jet printed samples from gas- and water-atomized alloy 625 powders journal February 2017
Calibration of the discrete element method and the effect of particle shape journal September 2016
Method for characterization and enhancement of 3D printing by binder jetting applied to the textures quality journal April 2017
Brief data overview of differently heat treated binder jet printed samples made from argon atomized alloy 625 powder journal December 2016
Fragmentation and restructuring of soft-agglomerates under shear journal February 2010
Solid oxide fuel cell technology?features and applications journal October 2004
Micro–macro simulation of sintering process by coupling Monte Carlo and finite element methods journal June 2004
Comparison of Linear and 4-Arm Star Poly(vinyl pyrrolidone) for Aqueous Binder Jetting Additive Manufacturing of Personalized Dosage Tablets journal June 2019
Development and Design of Binder Systems for Titanium Metal Injection Molding: An Overview journal October 2012
Tracking Global Growth in Industrial-Scale Additive Manufacturing journal March 2014
Drop spreading and penetration into pre-wetted powders journal May 2013
Improving accuracy of powder‐based SFF processes by metal deposition from a nanoparticle dispersion journal October 2006
An exploration of binder jetting of copper journal March 2015
Fabrication of Metal and Alloy Components by Additive Manufacturing: Examples of 3D Materials Science journal April 2012
Densification and shape retention in supersolidus liquid phase sintering journal December 1999
Development of a new calcium phosphate powder-binder system for the 3D printing of patient specific implants journal January 2007
Fabrication of Functionally Gradient Ultrafine-Grained WC-Co Composites journal September 2013
Numerical simulation of dynamic contact angle using a force based formulation journal September 2011
Densification and Properties of 420 Stainless Steel Produced by Three-Dimensional Printing With Addition of Si3N4 Powder journal October 2009
A robust process optimization for a powder type rapid prototyper journal August 2002
Additive manufacturing and sustainability: an exploratory study of the advantages and challenges journal November 2016
Lattice Boltzmann study on the dynamics of successive droplets impact on a solid surface journal May 2016
Binder jetting additive manufacturing of 420 stainless steel: Densification during sintering and effect of heat treatment on microstructure and hardness journal January 2020
Solid free-form fabrication of drug delivery devices journal June 1996
Effect of solutionizing and aging on the microstructure and mechanical properties of powder bed binder jet printed nickel-based superalloy 625 journal December 2016
Effects of thermal treatments on microstructure and mechanical properties of a Co–Cr–Mo–W biomedical alloy produced by laser sintering journal July 2016
Effect of heat-treatment temperature on microstructures and mechanical properties of Co–Cr–Mo alloys fabricated by selective laser melting journal May 2018
Martensitic transformation, mechanical property and magnetic-field-induced strain of Ni–Mn–Ga alloy fabricated by spark plasma sintering journal March 2011
Additive manufacturing: technology, applications and research needs journal May 2013
Design and characterisation of food grade powders and inks for microstructure control using 3D printing journal March 2018
Economic implications of 3D printing: Market structure models in light of additive manufacturing revisited journal June 2015
3D printing using concrete extrusion: A roadmap for research journal October 2018
Critical success factors for adoption of 3D printing journal July 2018
A review on 3D printed bioimplants journal May 2015
Novel processing of iron–manganese alloy-based biomaterials by inkjet 3-D printing journal November 2013
Selective recrystallization of cellulose composite powders and microstructure creation through 3D binder jetting journal November 2018
Fabrication of porous silicon nitride ceramics using binder jetting technology journal July 2016
Microstructure and properties of Ni–Mn–Ga alloys produced by rapid solidification and pulsed electric current sintering journal May 2011
Effect of binder content on the material properties of polymethyl methacrylate fabricated by three dimensional printing technique journal October 2008
Properties of as-deposited and heat-treated Ni-Mn-Ga magnetic shape memory alloy processed by directed energy deposition journal July 2018
Magnetocaloric Effect in Ni–Mn–Ga Alloys journal November 2008
Influence of Cutting Parameters and Tool Wear on the Surface Integrity of Cobalt-Based Stellite 6 Alloy When Machined Under a Dry Cutting Environment journal November 2016
Cytocompatibility of brushite and monetite cell culture scaffolds made by three-dimensional powder printing journal February 2009
Binder droplet impact mechanism on a hydroxyapatite microsphere surface in 3D printing of bone scaffolds journal April 2015
Moisture based three-dimensional printing of calcium phosphate structures for scaffold engineering journal February 2013
Binder jetting of ceramics: Powders, binders, printing parameters, equipment, and post-treatment journal July 2019
Investigation of Sintering Shrinkage in Binder Jetting Additive Manufacturing Process journal January 2017
Toward 3D Printed Bioactive Titanium Scaffolds with Bimodal Pore Size Distribution for Bone Ingrowth journal January 2013
On the influence of sintering protocols and layer thickness on the physical and mechanical properties of additive manufactured titanium porous bio-structures journal December 2016
Discrete element simulation and experimental study of powder spreading process in additive manufacturing journal January 2017
The role of particle size on the laser sintering of iron powder journal October 2004
Fabrication of SiC whisker-reinforced SiC ceramic matrix composites based on 3D printing and chemical vapor infiltration technology journal September 2019
Additive manufacturing: scientific and technological challenges, market uptake and opportunities journal January 2018
Powder bed binder jet printed alloy 625: Densification, microstructure and mechanical properties journal October 2016
Small-scale free surface flows with breakup: Drop formation and emerging applications journal September 2002
Wettability and spreading kinetics of Al and Mg on TiC journal June 2003
Characterizing Binder–Powder Interaction in Binder Jetting Additive Manufacturing Via Sessile Drop Goniometry journal October 2018
Electron Microscopy Investigation of Binder Saturation and Microstructural Defects in Functional Parts Made by Additive Manufacturing journal July 2016
Nickel base superalloy GH4049 prepared by powder metallurgy journal April 2009
Effects of Hot Isostatic Pressing on Copper Parts Fabricated via Binder Jetting journal January 2017
Particle-based simulation of powder application in additive manufacturing journal January 2016
Microstructure and tensile properties optimization of MIM418 superalloy by heat treatment journal January 2016
Three-dimensional printing of metal parts for tooling and other applications journal November 2000
An accurate and efficient tangential force–displacement model for elastic frictional contact in particle-flow simulations journal April 1999
Free Energy of a Nonuniform System. I. Interfacial Free Energy journal February 1958
Additive manufacturing of biomaterials journal April 2018
Recent advances in 3D printing of porous ceramics: A review journal December 2017
Binder-Jet Printing of Fine Stainless Steel Powder with Varied Final Density journal November 2016
Manufacturing and characterization of porous titanium components journal September 2014
Solid State Sintered 3-D Printing Component by Using Inkjet (Binder) Method journal January 2016
Process limitations of 3D printing model rock journal April 2018
Evaluation of 3D printing for dies in low volume forging of 7075 aluminum helicopter parts journal December 2005
3D printing of porous hydroxyapatite scaffolds intended for use in bone tissue engineering applications journal February 2015
The cross-disciplinary emergence of 3D printed bioceramic scaffolds in orthopedic bioengineering journal January 2018
Microstructure, phase transformation and mechanical property of Ni–Mn–Ga particles/Mg composites journal October 2014
Computer modeling and simulation of solid-state sintering: A phase field approach journal February 2006
The effect of aging treatment on the fracture toughness and impact strength of injection molded Ni-625 superalloy parts journal October 2015
Process development toward full-density stainless steel parts with binder jetting printing journal October 2017
Selective laser melting of La(Fe,Co,Si) 13 geometries for magnetic refrigeration journal July 2013
Why Magnetic Shape Memory Alloys? journal June 2012
Obtaining desired surface roughness of castings produced using ZCast direct metal casting process through Taguchi's experimental approach journal September 2012
3D printing of Al2O3/Cu–O interpenetrating phase composite journal September 2010
Inkjet-Printed Line Morphologies and Temperature Control of the Coffee Ring Effect journal March 2008
Porous bioceramics produced by inkjet 3D printing: Effect of printing ink formulation on the ceramic macro and micro porous architectures control journal December 2018
Microstructural and mechanical properties of injection moulded gas and water atomised 17-4 PH stainless steel powder journal June 2007
Effect of Lattice Design and Process Parameters on Dimensional and Mechanical Properties of Binder Jet Additively Manufactured Stainless Steel 316 for Bone Scaffolds journal January 2017
Segregation of titanium powder with polydisperse size distribution: Spectral and correlation analyses journal March 2015
Wetting, disintegration and dissolution of agglomerated water soluble powders journal January 2011
Acoustic emission technique used for detecting early stages of precipitation during aging of Inconel 625 journal December 2003
Effects of silica and zinc oxide doping on mechanical and biological properties of 3D printed tricalcium phosphate tissue engineering scaffolds journal February 2012
High Speed Imaging and Analysis of Jet and Drop Formation journal January 2007
Sintering regimes and resulting microstructure and properties of binder jet 3D printed Ni-Mn-Ga magnetic shape memory alloys journal August 2018
Fatigue behavior of highly porous titanium produced by powder metallurgy with temporary space holders journal March 2016
Process Development of Porcelain Ceramic Material with Binder Jetting Process for Dental Applications journal January 2016
Atomization process for metal powder journal October 2004
Ni-Mn-Ga micro-trusses via sintering of 3D-printed inks containing elemental powders journal January 2018
Size Effects on Magnetic Actuation in Ni-Mn-Ga Shape-Memory Alloys journal October 2010
Microstructural evolution and magnetic properties of binder jet additive manufactured Ni-Mn-Ga magnetic shape memory alloy foam journal June 2017
Effect of oxides on binder burnout during ceramics processing journal June 1989
Powder-spreading mechanisms in powder-bed-based additive manufacturing: Experiments and computational modeling journal October 2019
Effects of compaction pressure and particle shape on the porosity and compression mechanical properties of sintered Ti6Al4V powder compacts for hard tissue implantation journal January 2008
Direct numerical simulation of gas-solid-liquid flows with capillary effects: An application to liquid bridge forces between spherical particles journal December 2016
Powder bed binder jet 3D printing of Inconel 718: Densification, microstructural evolution and challenges☆ journal August 2017
Giant magnetic-field-induced strains in polycrystalline Ni–Mn–Ga foams journal September 2009
Sharp interface immersed-boundary/level-set method for wave–body interactions journal September 2009
Material characteristics of binder jet 3D printed hydrated CSA cement with the addition of fine aggregates journal May 2019
Microstructural evolution of injection molded gas- and water-atomized 316L stainless steel powder during sintering journal January 2005
Understanding in vivo response and mechanical property variation in MgO, SrO and SiO2 doped β-TCP journal June 2011
Modeling of infiltration kinetics for liquid metal processing of composites journal February 1988
Fundamental Study on Applicability of Powder-Based 3D Printer for Physical Modeling in Rock Mechanics journal January 2016
Ink-Jet Printing of Binders for Ceramic Components journal April 2002
Drop penetration time in heterogeneous powder beds journal December 2009
Critical influences of particle size and adhesion on the powder layer uniformity in metal additive manufacturing journal April 2019
The need for Powder Characterisation in the Additive Manufacturing Industry and the Establishment of a National Facility journal August 2015
Optimization of Binder Jetting Using Taguchi Method journal January 2017
Open-cellular copper structures fabricated by additive manufacturing using electron beam melting journal June 2011
A continuum method for modeling surface tension journal June 1992
The metallurgy and processing science of metal additive manufacturing journal March 2016
The determination of the mechanism of sintering journal February 1967
Methods for Minimizing Segregation: A Review journal October 2004
Interface- and diffusion-limited capillary rise of reactive melts with a transient contact angle journal July 2002
Metal Additive Manufacturing: A Review journal April 2014
Mechanical Properties of the Stellite 6 Cobalt Alloy Implanted with Nitrogen Ions journal August 2017
Discrete element method simulation of cohesive particles mixing under magnetically assisted impaction journal July 2013
Binder Jet Printed Iron Silicon with Low Hysteresis Loss conference May 2019
Direct 3D powder printing of biphasic calcium phosphate scaffolds for substitution of complex bone defects journal January 2014
Tailor-made tricalcium phosphate bone implant directly fabricated by a three-dimensional ink-jet printer journal December 2006
A review on powder-based additive manufacturing for tissue engineering: selective laser sintering and inkjet 3D printing journal June 2015
Numerical studies of droplet splashing on a dry surface: triggering a splash with the dynamic contact angle journal January 2011
Hydrophobic/hydrophilic static powder beds: Competing horizontal spreading and vertical imbibition mechanisms of a single droplet journal May 2018
Inkjet printing - the physics of manipulating liquid jets and drops journal March 2008
The stability of ink-jet printed lines of liquid with zero receding contact angle on a homogeneous substrate journal February 2003
Characterization of Gas Atomized Ni-Mn-Ga Powders journal January 2015
Magnetic field induced strain and damping behavior of Ni–Mn–Ga particles/epoxy resin composite journal August 2014
A three-dimensional osteochondral composite scaffold for articular cartilage repair journal December 2002
Self-patterning of epitaxial Ni–Mn–Ga/MgO(001) thin films journal June 2016
Contact angle hysteresis: a review of fundamentals and applications journal September 2012
Selective laser melting additive manufactured Inconel 718 superalloy parts: High-temperature oxidation property and its mechanisms journal October 2014
Fabrication of Al2O3-based composites by indirect 3D-printing journal February 2006
Flow mechanisms in high pressure gas atomization journal November 1991
On two-phase flow solvers in irregular domains with contact line journal September 2016
Functionally graded material of 304L stainless steel and inconel 625 fabricated by directed energy deposition: Characterization and thermodynamic modeling journal April 2016
Microstructure characteristics and fractal analysis of 3D-printed sandstone using micro-CT and SEM-EDS journal April 2019
Sensing mechanism of a porous ceramic as humidity sensor journal July 1999
Sintering of 3D-Printed Glass/HAp Composites journal July 2012
Mechanical properties of porous titanium compacts prepared by powder sintering journal December 2003
A study of the evolution of microstructure and consolidation kinetics during sintering using a phase field modeling based approach journal June 2016
Microstructure and porosity evolution during sintering of Ni-Mn-Ga wires printed from inks containing elemental powders journal January 2019
Segregation of Particulate Materials – Mechanisms and Testers journal January 1996
Lattice Misfit Measurement in Inconel 625 by X-Ray Diffraction Technique journal September 2008
Numerical simulation of particle–particle adhesion by dynamic liquid bridge journal December 2015
Modeling morphology evolution and densification during solid-state sintering via kinetic Monte Carlo simulation journal October 2016
A new approach for fabrication of titanium-titanium boride periodic composite via additive manufacturing and pressure-less sintering journal April 2018
Characterization and Control of Nanoparticle Emission during 3D Printing journal August 2017

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