All-diamond optical assemblies for a beam-multiplexing X-ray monochromator at the Linac Coherent Light Source

Stoupin, S.; Terentyev, S. A.; Blank, V. D.; Shvyd'ko, Yu. V.; Goetze, K.; Assoufid, L.; Polyakov, S. N.; Kuznetsov, M. S.; Kornilov, N. V.; Katsoudas, J.; Alonso-Mori, R.; Chollet, M.; Feng, Y.; Glownia, J. M.; Lemke, H.; Robert, A.; Sikorski, M.; Song, S.; Zhu, D.

doi:10.1107/s1600576714013028

All-diamond optical assemblies for a beam-multiplexing X-ray monochromator at the Linac Coherent Light Source

Journal Article · Fri Aug 01 00:00:00 EDT 2014 · Journal of Applied Crystallography (Online)

DOI:https://doi.org/10.1107/s1600576714013028· OSTI ID:1625766

Stoupin, S. ^[1]; Terentyev, S. A. ^[2]; Blank, V. D. ^[2]; Shvyd'ko, Yu. V. ^[3]; Goetze, K. ^[3]; Assoufid, L. ^[3]; Polyakov, S. N. ^[4]; Kuznetsov, M. S. ^[2]; Kornilov, N. V. ^[2]; Katsoudas, J. ^[5]; Alonso-Mori, R. ^[6]; Chollet, M. ^[6]; Feng, Y. ^[6]; Glownia, J. M. ^[6]; Lemke, H. ^[6]; Robert, A. ^[6]; Sikorski, M. ^[6]; Song, S. ^[6]; Zhu, D. ^[6]

Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS); DOE/OSTI
Technological Inst. for Superhard and Novel Carbon Materials, Troitsk (Russian Federation)
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Technological Inst. for Superhard and Novel Carbon Materials, Troitsk (Russian Federation); Lomonsov Moscow State Univ. (Russian Federation). Skobeltsyn Inst. of Nuclear Physics
Illinois Institute of Technology, Chicago, IL (United States)
SLAC National Accelerator Lab., Menlo Park, CA (United States). Linac Coherent Light Source (LCLS)

A double-crystal diamond (111) monochromator recently implemented at the Linac Coherent Light Source (LCLS) enables splitting of the primary X-ray beam into a pink (transmitted) and a monochromatic (reflected) branch. The first monochromator crystal, with a thickness of ~100 µm, provides sufficient X-ray transmittance to enable simultaneous operation of two beamlines. This article reports the design, fabrication and X-ray characterization of the first and second (300 µm-thick) crystals utilized in the monochromator and the optical assemblies holding these crystals. Each crystal plate has a region of about 5 × 2 mm with low defect concentration, sufficient for use in X-ray optics at the LCLS. The optical assemblies holding the crystals were designed to provide mounting on a rigid substrate and to minimize mounting-induced crystal strain. The induced strain was evaluated using double-crystal X-ray topography and was found to be small over the 5 × 2 mm working regions of the crystals.

View Accepted Manuscript (DOE)

Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); Russian Ministry of Education and Science

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1625766

Journal Information:: Journal of Applied Crystallography (Online), Journal Name: Journal of Applied Crystallography (Online) Journal Issue: 4 Vol. 47; ISSN 1600-5767; ISSN JACGAR

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: United States

Language:: English

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Short-wavelength free-electron laser sources and science: a review Seddon, E. A.; Clarke, J. A.; Dunning, D. J. Reports on Progress in Physics, Vol. 80, Issue 11 https://doi.org/10.1088/1361-6633/aa7cca	journal	October 2017
Output coupling from x-ray free-electron laser cavities with intracavity beam splitters Shvyd’ko, Yuri Physical Review Accelerators and Beams, Vol. 22, Issue 10 https://doi.org/10.1103/physrevaccelbeams.22.100703	journal	October 2019
Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source Feng, Y.; Alonso-Mori, R.; Barends, T. R. M. Journal of Synchrotron Radiation, Vol. 22, Issue 3 https://doi.org/10.1107/s1600577515003999	journal	April 2015
Single-crystal diamond refractive lens for focusing X-rays in two dimensions Antipov, S.; Baryshev, S. V.; Butler, J. E. Journal of Synchrotron Radiation, Vol. 23, Issue 1 https://doi.org/10.1107/s1600577515020639	journal	January 2016
Linear parabolic single-crystal diamond refractive lenses for synchrotron X-ray sources Terentyev, Sergey; Polikarpov, Maxim; Snigireva, Irina Journal of Synchrotron Radiation, Vol. 24, Issue 1 https://doi.org/10.1107/s1600577516017331	journal	January 2017
Probing Dynamics in Colloidal crystals with pump-probe experiments at LCLS Methodololgy and analysis Vartaniants, Ivan; Mukharamova, Nastsia; Lazarev, Sergey Deutsches Elektronen-Synchrotron, DESY, Hamburg https://doi.org/10.3204/pubdb-2017-03368	text	January 2017
Short-wavelength free-electron laser sources and science: a review Seddon, E. A.; Clarke, J. A.; Dunning, D. J. Deutsches Elektronen-Synchrotron, DESY, Hamburg https://doi.org/10.3204/pubdb-2018-00596	text	January 2017
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Output coupling from x-ray free-electron laser cavities with intracavity beam splitters Shvyd'ko, Yuri arXiv https://doi.org/10.48550/arxiv.1906.09509	text	January 2019

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