A hard X-ray nanoprobe beamline for nanoscale microscopy

Winarski, Robert P.; Holt, Martin V.; Rose, Volker; Fuesz, Peter; Carbaugh, Dean; Benson, Christa; Shu, Deming; Kline, David; Stephenson, G. Brian; McNulty, Ian; Maser, Jörg

doi:10.1107/s0909049512036783

A hard X-ray nanoprobe beamline for nanoscale microscopy

Journal Article · Wed Sep 05 00:00:00 EDT 2012 · Journal of Synchrotron Radiation

DOI:https://doi.org/10.1107/s0909049512036783· OSTI ID:1625703

Winarski, Robert P. ^[1]; Holt, Martin V. ^[2]; Rose, Volker ^[3]; Fuesz, Peter ^[4]; Carbaugh, Dean ^[2]; Benson, Christa ^[4]; Shu, Deming ^[4]; Kline, David ^[4]; Stephenson, G. Brian ^[4]; McNulty, Ian ^[2]; Maser, Jörg ^[3]

Argonne National Lab. (ANL), Argonne, IL (United States). Center for Nanoscale Materials; DOE/OSTI
Argonne National Lab. (ANL), Argonne, IL (United States). Center for Nanoscale Materials
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS). Center for Nanoscale Materials
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

The Hard X-ray Nanoprobe Beamline (or Nanoprobe Beamline) is an X-ray microscopy facility incorporating diffraction, fluorescence and full-field imaging capabilities designed and operated by the Center for Nanoscale Materials and the Advanced Photon Source at Sector 26 of the Advanced Photon Source at Argonne National Laboratory. This facility was constructed to probe the nanoscale structure of biological, environmental and material sciences samples. The beamline provides intense focused X-rays to the Hard X-ray Nanoprobe (or Nanoprobe) which incorporates Fresnel zone plate optics and a precision laser sensing and control system. The beamline operates over X-ray energies from 3 to 30 keV, enabling studies of most elements in the periodic table, with a particular emphasis on imaging transition metal

View Accepted Manuscript (DOE)

Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1625703

Journal Information:: Journal of Synchrotron Radiation, Journal Name: Journal of Synchrotron Radiation Journal Issue: 6 Vol. 19; ISSN 0909-0495; ISSN JSYRES

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: United States

Language:: English

References (27)

Real-time X-ray Investigation of Aluminum Foam Sandwich Production Banhart, J.; Stanzick, H.; Helfen, L. Advanced Engineering Materials, Vol. 3, Issue 6 https://doi.org/10.1002/1527-2648(200106)3:6<407::AID-ADEM407>3.0.CO;2-Y	journal	June 2001
Advances in nanomagnetism via X-ray techniques Srajer, G.; Lewis, L. H.; Bader, S. D. Journal of Magnetism and Magnetic Materials, Vol. 307, Issue 1 https://doi.org/10.1016/j.jmmm.2006.06.033	journal	December 2006
Combining scanning tunneling microscopy and synchrotron radiation for high-resolution imaging and spectroscopy with chemical, electronic, and magnetic contrast Cummings, M. L.; Chien, T. Y.; Preissner, C. Ultramicroscopy, Vol. 112, Issue 1 https://doi.org/10.1016/j.ultramic.2011.09.018	journal	January 2012
Development of a Hard X–ray Nanoprobe Beamline at the Advanced Photon Source Maser, J.; Stephenson, B.; Winarski, R. Microscopy and Microanalysis, Vol. 11, Issue S02 https://doi.org/10.1017/S1431927605505191	journal	August 2005
Observation of five-fold local symmetry in liquid lead Reichert, H.; Klein, O.; Dosch, H. Nature, Vol. 408, Issue 6814 https://doi.org/10.1038/35048537	journal	December 2000
Bragg transmission phase plates for the production of circularly polarized x rays Lang, J. C.; Srajer, George Review of Scientific Instruments, Vol. 66, Issue 2 https://doi.org/10.1063/1.1145902	journal	February 1995
APS undulator radiation—first results Cai, Z.; Dejus, R. J.; Den Hartog, P. Review of Scientific Instruments, Vol. 67, Issue 9 https://doi.org/10.1063/1.1147262	journal	September 1996
Performance of a double-multilayer monochromator at Beamline 2-BM at the Advanced Photon Source Chu, Y. S.; Liu, C.; Mancini, D. C. Review of Scientific Instruments, Vol. 73, Issue 3 https://doi.org/10.1063/1.1423628	journal	March 2002
A unique polarized x-ray facility at the Advanced Photon Source Freeland, J. W.; Lang, J. C.; Srajer, G. Review of Scientific Instruments, Vol. 73, Issue 3 https://doi.org/10.1063/1.1435814	journal	March 2002
White Beam Slits and Pink Beam Slits for the Hard X-ray Nanoprobe Beamline at the Advanced Photon Source Benson, C.; Jaski, Y.; Maser, J. SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings https://doi.org/10.1063/1.2436246	conference	January 2007
Optomechanical Design of a Hard X-ray Nanoprobe Instrument with Nanometer-Scale Active Vibration Control Shu, D.; Maser, J.; Holt, M. SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings https://doi.org/10.1063/1.2436307	conference	January 2007
X-ray nanotomography of SiO ₂ -coated Pt ₉₀ Ir ₁₀ tips with sub-micron conducting apex Rose, V.; Chien, T. Y.; Hiller, J. Applied Physics Letters, Vol. 99, Issue 17 https://doi.org/10.1063/1.3655907	journal	October 2011
The history and future of X-ray microscopy Kirz, J.; Jacobsen, C. Journal of Physics: Conference Series, Vol. 186 https://doi.org/10.1088/1742-6596/186/1/012001	journal	September 2009
On the Phase-Contrast Test of F. Zernike Burch, C. R.; Stratton, F. J. M. Monthly Notices of the Royal Astronomical Society, Vol. 94, Issue 5 https://doi.org/10.1093/mnras/94.5.384	journal	March 1934
Absorption of circularly polarized x rays in iron Schütz, G.; Wagner, W.; Wilhelm, W. Physical Review Letters, Vol. 58, Issue 7 https://doi.org/10.1103/PhysRevLett.58.737	journal	February 1987
X-Ray Natural Circular Dichroism Alagna, Lucilla; Prosperi, Tommaso; Turchini, Stefano Physical Review Letters, Vol. 80, Issue 21 https://doi.org/10.1103/PhysRevLett.80.4799	journal	May 1998
Dynamical Diffraction of X Rays by Perfect Crystals Batterman, Boris W.; Cole, Henderson Reviews of Modern Physics, Vol. 36, Issue 3 https://doi.org/10.1103/RevModPhys.36.681	journal	July 1964
Three-dimensional maps of grain boundaries and the stress state of individual grains in polycrystals and powders Poulsen, H. F.; Nielsen, S. F.; Lauridsen, E. M. Journal of Applied Crystallography, Vol. 34, Issue 6 https://doi.org/10.1107/S0021889801014273	journal	November 2001
X-ray microscopy Sayre, D.; Chapman, H. N. Acta Crystallographica Section A Foundations of Crystallography, Vol. 51, Issue 3 https://doi.org/10.1107/S0108767394011803	journal	May 1995
A fast mechanical shutter for submicrosecond time-resolved synchrotron experiments Gembicky, Milan; Oss, Dan; Fuchs, Ryan Journal of Synchrotron Radiation, Vol. 12, Issue 5 https://doi.org/10.1107/S090904950501770X	journal	August 2005
Nanofabrication of high aspect ratio 24 nm x-ray zone plates for x-ray imaging applications Feng, Yan; Feser, Michael; Lyon, Alan Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures, Vol. 25, Issue 6 https://doi.org/10.1116/1.2789447	journal	January 2007
Watching a Protein as it Functions with 150-ps Time-Resolved X-ray Crystallography Schotte, F. Science, Vol. 300, Issue 5627 https://doi.org/10.1126/science.1078797	journal	June 2003
The Structure of the Potassium Channel: Molecular Basis of K+ Conduction and Selectivity Doyle, D. A. Science, Vol. 280, Issue 5360 https://doi.org/10.1126/science.280.5360.69	journal	April 1998
Ellipsoidal and parabolic glass capillaries as condensers for x-ray microscopes Zeng, Xianghui; Duewer, Fred; Feser, Michael Applied Optics, Vol. 47, Issue 13 https://doi.org/10.1364/AO.47.002376	journal	January 2008
Phase zone plates for x rays and the extreme uv Kirz, Janos Journal of the Optical Society of America, Vol. 64, Issue 3 https://doi.org/10.1364/JOSA.64.000301	journal	January 1974
Two dimensional hard x-ray nanofocusing with crossed multilayer Laue lenses Yan, Hanfei; Rose, Volker; Shu, Deming Optics Express, Vol. 19, Issue 16 https://doi.org/10.1364/OE.19.015069	journal	January 2011
X-ray computed tomography in Zernike phase contrast mode at 8 keV with 50-nm resolution using Cu rotating anode X-ray source Tkachuk, Andrei; Duewer, Fred; Cui, Hongtao Zeitschrift für Kristallographie - Crystalline Materials, Vol. 222, Issue 11/2007 https://doi.org/10.1524/zkri.2007.222.11.650	journal	January 2007

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A hard X-ray nanoprobe beamline for nanoscale microscopy

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