Solid-state synthesis of ordered mesoporous carbon catalysts via a mechanochemical assembly through coordination cross-linking

Zhang, Pengfei; Wang, Li; Yang, Shize; Schott, Jennifer A.; Liu, Xiaofei; Mahurin, Shannon M.; Huang, Caili; Zhang, Yu; Fulvio, Pasquale F.; Chisholm, Matthew F.; Dai, Sheng

doi:10.1038/ncomms15020

Title: Solid-state synthesis of ordered mesoporous carbon catalysts via a mechanochemical assembly through coordination cross-linking

Journal Article · Fri Apr 28 00:00:00 EDT 2017 · Nature Communications

DOI:https://doi.org/10.1038/ncomms15020· OSTI ID:1623886

^[1]; Wang, Li ^[2];

^[3]; Schott, Jennifer A. ^[4]; Liu, Xiaofei ^[5]; Mahurin, Shannon M. ^[1]; Huang, Caili ^[6]; Zhang, Yu ^[7];

^[8]; Chisholm, Matthew F. ^[3];

^[4]

Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division; East China Univ. of Science and Technology, Shanghai (China). Key Laboratory for Advanced Materials and Research Institute of Industrial Catalysis
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science and Technology Division
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Chemical Sciences Division; Univ. of Tennessee, Knoxville, TN (United States). Dept. of Chemistry
East China Univ. of Science and Technology, Shanghai (China). Key Laboratory for Advanced Materials and Research Institute of Industrial Catalysis
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Science Directorate
Vanderbilt Univ., Nashville, TN (United States). Dept. of Chemical and Biomolecular Engineering
Univ. of Puerto Rico, San Juan, PR (United States). Dept. of Chemistry

Ordered mesoporous carbons (OMCs) have demonstrated great potential in catalysis, and as supercapacitors and adsorbents. Since the introduction of the organic–organic self-assembly approach in 2004/2005 until now, the direct synthesis of OMCs is still limited to the wet processing of phenol-formaldehyde polycondensation, which involves soluble toxic precursors, and acid or alkali catalysts, and requires multiple synthesis steps, thus restricting the widespread application of OMCs. Herein, we report a simple, general, scalable and sustainable solid-state synthesis of OMCs and nickel OMCs with uniform and tunable mesopores (~4–10 nm), large pore volumes (up to 0.96 cm³ g^–1) and high-surface areas exceeding 1,000m²g^–1, based on a mechanochemical assembly between polyphenol-metal complexes and triblock co-polymers. Nickel nanoparticles (~5.40nm) confined in the cylindrical nanochannels show great thermal stability at 600 °C. Moreover, the nickel OMCs offer exceptional activity in the hydrogenation of bulky molecules (~2 nm).

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division; National Basic Research Program of China; National High Technology Research and Development Program of China; USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1623886

Journal Information:: Nature Communications, Vol. 8, Issue 1; ISSN 2041-1723

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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