skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Characterization of Inconel 625 fabricated using powder-bed-based additive manufacturing technologies

Journal Article · · Journal of Materials Processing Technology

The purpose of this study was to perform a comparative analysis of powder-bed-based additive manufacturing (AM) technologies during the production of metallic components using Inconel 625 powder material. The AM technologies explored in this study include electron beam powder bed fusion (EPBF), laser powder bed fusion (LPBF), and binder jetting technology. Samples were fabricated in two build directions (X and Z build orientations) for this evaluation process, where all specimens underwent a hot isostatic pressing (HIP) post-process. The comparison was made in terms of microstructure and mechanical properties including ultimate tensile strength (UTS), yield strength (YS), percent elongation, and modulus of elasticity (E). Microstructural characterization showed evidence of equiaxed grain formation for binder jetting and LPBF parts, whereas EPBF parts displayed a more columnar grain formation parallel to the build direction. Six specimens were tested per technology, three built in the X orientation and three built in the Z orientation. All six specimens were built in a single run of each AM machine. Results indicated that all three technologies are capable of meeting the minimum requirements of the ASTM F3056-14 standard for parts produced in the X orientation, with properties that are similar to wrought Inconel 625. In the Z orientation, however, only LPBF was able to meet the minimum standard requirements. Through the comparative analysis of the mechanical properties, here this work showed that LPBF outperformed the other technologies in a majority of the evaluated properties, followed by EPBF and binder jetting. An analysis of the fracture surfaces of tensile specimens was also performed, and it indicated ductile fracture (dimple rupture) for the specimens produced with all three of the AM technologies studied. Nevertheless, the characterization also showed certain differences in the fractured surfaces, such as the presence of un-sintered powder particles for the binder jetting processed Inconel 625, or the development of the so called woody structure for the EPBF processed material. This study can be used to determine distinct characteristics between the three powder-bed-based technologies for the fabrication of Inconel 625 that can further include other technologies and materials using similar approaches.

Research Organization:
Univ. of Texas at El Paso, TX (United States)
Sponsoring Organization:
USDOE Office of Fossil Energy (FE)
Grant/Contract Number:
FE0012321
OSTI ID:
1614183
Alternate ID(s):
OSTI ID: 1702812
Journal Information:
Journal of Materials Processing Technology, Vol. 264, Issue C; ISSN 0924-0136
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 90 works
Citation information provided by
Web of Science

References (21)

High Power Selective Laser Melting (HP SLM) of Aluminum Parts journal January 2011
Tool-life and wear mechanisms of CBN tools in machining of Inconel 718 journal June 2007
Experimental investigation of process parameters on layer thickness and density in direct metal laser sintering: a response surface methodology approach journal March 2017
Fabrication of barium titanate by binder jetting additive manufacturing technology journal June 2015
Hall–Petch relation and boundary strengthening journal October 2004
Comparison of Inconel 625 and Inconel 600 in resistance to cavitation erosion and jet impingement erosion journal October 2010
Influence of SLM process parameters on the surface finish, porosity rate and fatigue behavior of as-built Inconel 625 parts journal May 2018
Selective laser melting of iron-based powder journal June 2004
The microstructure evolution and nucleation mechanisms of dynamic recrystallization in hot-deformed Inconel 625 superalloy journal February 2011
Properties of Inconel 625 mesh structures grown by electron beam additive manufacturing journal October 2014
Influence of heat treatments on microstructure evolution and mechanical properties of Inconel 625 processed by laser powder bed fusion journal June 2018
Powder bed binder jet printed alloy 625: Densification, microstructure and mechanical properties journal October 2016
Effect of solutionizing and aging on the microstructure and mechanical properties of powder bed binder jet printed nickel-based superalloy 625 journal December 2016
Microstructural evolution and mechanical properties of differently heat-treated binder jet printed samples from gas- and water-atomized alloy 625 powders journal February 2017
Top surface and side roughness of Inconel 625 parts processed using selective laser melting journal March 2009
Characteristics of Inconel Powders for Powder-Bed Additive Manufacturing journal October 2017
Satellite formation mechanism in gas atomised powders journal January 1999
Effect of precipitation on post-heat-treated Inconel 625 alloy after friction stir welding journal June 2010
Powder flowability characterisation methodology for powder-bed-based metal additive manufacturing journal July 2015
Powder characterisation techniques and effects of powder characteristics on part properties in powder-bed fusion processes journal December 2016
Surface Reactions During Water Atomisation and Sintering of Austenitic Stainless Steel Powder journal January 1995

Cited By (2)

Mechanical and microstructural characterization of arc-welded inconel 625 alloy text January 2019
Analysis of the Machining Process of Inconel 718 Parts Manufactured by Laser Metal Deposition journal July 2019